Author Topic: KX Reference  (Read 94430 times)

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Offline CalMachineTopic starter

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KX Reference
« on: May 14, 2017, 04:09:55 pm »
Rather than further digging the hole, that is the 80-page LTZ1000 thread, I've decided to start a new thread for any members to showcase their KX references designed by TiN!

This weekend I was able to assemble everything, but 1 component, on 1 of my KX references.  Somehow I overlooked the 22 nF cap when placing my order from Digikey... so I will have to wait a few days for that to arrive until it is finished and I can start monitoring.  I am still really new to SMD soldering, so just assembling this board took me several hours.  I didn't leave my iron on for more than 2 or 3 seconds before removing heat and applied cooling.  I used tweezers/forceps for extra heat dissipation where applicable and the solder I used was SN62/PB36/AG2

I purchased Vishay 'black magic' resistors for both my my KX boards, but I decided to get some PWW resistors from Edwin for my 2nd KX reference.

Major components ready to go!


Clean board ready to be assembled.


Components from Digikey... sadly there is no 22 nF caps in there  :--
[/url]

Small surface mount resistors were put on first.


First AZ OP and caps put into place


Second AZ OP and MAX temp sensor put in place
[/url]

Getting the magical resistors in place!  Also, the underside MAX Temp sensor was put in place prior to this.  I had forgotten to take a picture at that step.


Heater resistors and Zener current resistors are in.  There was no way these metal enclosures were going to fit side by side, so I had to improvise slightly.  I am not certain, but I feel like my solution was a pretty good one.  I did not have to bend leads much.  Once one resistor was in the holes to the approximate depth I was looking for, I grabbed the leads between the PCB and resistor body for support.  All stress of bending was put into the leads, and leads alone.  I've seen other members wrap some sort of foil or something around the heater pair for increased thermal coupling.  I will most likely end up doing something similar to that once I figure out what I want to do.


LTZ1000 tac'd down!  Man... I've never been more nervous or scared while soldering, in my life!  Nothing like getting your blood pumping, than soldering on a $50 component for the first time.


The underside after soldering.


Tada!!!!!










Here is a little glass dome that I was wanting to help keep the LTZ1000 at thermal equilibrium as well as isolated from any air movement.  Although,  I've read that TOO much isolation can be bad.  I would like to hear opinions on a small little glass dome, such as this one.





I would love to hear any questions/comments/concerns regarding this board.  I am still a very novice VoltNut, so any advice would be greatly appreciated :)
« Last Edit: May 19, 2017, 12:15:46 am by CalMachine »
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Offline TiN

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Re: KX Reference
« Reply #1 on: May 14, 2017, 04:18:02 pm »
Glass dome is cool, where you got it? Too much insulation might be case for LM399, but for LTZ I wouldn't worry, there is enough thermal conductivity on FR4 board anyway.
I sense some hate rays were sent when assembling with those open guard traces, aye?

Check those film caps for shorts, it's VERY easy to destroy them by soldering.
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #2 on: May 14, 2017, 04:33:16 pm »
Glass dome is cool, where you got it? Too much insulation might be case for LM399, but for LTZ I wouldn't worry, there is enough thermal conductivity on FR4 board anyway.
I sense some hate rays were sent when assembling with those open guard traces, aye?

Check those film caps for shorts, it's VERY easy to destroy them by soldering.

I found the glass domes on flebay, actually.   I just made sure the internal dimensions were sufficient to house the LTZ1000 can.  They seem like they are almost a perfect fit!  I am still uncertain how I want to stick the dome to the board....  adhesive? little foam strip with small tie-down over the board?
http://www.ebay.com/itm/Hollow-Glass-Dome-for-Jewelry-10-5x19-5mm-Half-Dome-4-Pieces-/391731757716?

:-DD On multiple occasions I caught myself shouting "What the fuck?!"  :rant:  But in the end, I feel like it came out very well.   :phew:

I will definitely check the caps.  Those were probably one of the more difficult components to solder.  Somehow I managed to order the 1210 package for the 0.1 µF caps instead of the 1206...  so, that was fun!
« Last Edit: May 14, 2017, 05:04:44 pm by CalMachine »
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Offline ManateeMafia

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Re: KX Reference
« Reply #3 on: May 14, 2017, 05:33:16 pm »
Welcome to the KX LTZ club. Now you will have to make room somewhere and dedicate a meter to capturing data. xDevs will be wanting some ppm data soon.

I will be watching your progress. Edwin has an order from me so my project will be taking my time and money.
 

Online Kleinstein

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Re: KX Reference
« Reply #4 on: May 14, 2017, 07:36:40 pm »
The glass dome looks cool, but the whole thing should be inside a metal case anyway. So not much to see. Some (those made in larger quantities) glass ware is surprisingly cheap at the chemists supply.

When making a second version with PWW resistors, keep in mind the larger form factor - so it should use a different board layout, as bending the leads to much is not a good idea.
 

Offline Dr. Frank

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Re: KX Reference
« Reply #5 on: May 14, 2017, 07:58:14 pm »
The glass dome gives the LTZ1000 a nice look, as if it would be the kilogram prototype, Le Grand K.

Another thermal and air shield on the solder side would be much more important.

Frank
 

Offline CalMachineTopic starter

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Re: KX Reference
« Reply #6 on: May 14, 2017, 08:14:53 pm »
Welcome to the KX LTZ club. Now you will have to make room somewhere and dedicate a meter to capturing data. xDevs will be wanting some ppm data soon.

I will be watching your progress. Edwin has an order from me so my project will be taking my time and money.

I look forward to seeing how the reference performs  :-+   Right now, I've only got a Datron 1082 in my home lab for logging.  It's still a pretty phenomenal 7.5 digit meter with a DCV spec of ~10ppm/yr on the 10V range, but no 3458... 

I have yet to place my order with Edwin, I need a little bit of time to replenish funds.  :-DD


The glass dome gives the LTZ1000 a nice look, as if it would be the kilogram prototype, Le Grand K.

Another thermal and air shield on the solder side would be much more important.

Frank

I agree, I plan on having it reside in a die-cast aluminum enclosure for its life.  It might not be much to look at while it's in there, but outside it does look rather awesome! 

I've noticed other KX references with PWW resistors have some lead bending, and placement, that I am wanting to try to do... so with that said, I might rethink my KX referenced with PWW resistors.  I might just stick the Vishays in there and save the PWW resistors for my own design, instead of having 2 KX references with different resistor types.


The glass dome gives the LTZ1000 a nice look, as if it would be the kilogram prototype, Le Grand K.

Another thermal and air shield on the solder side would be much more important.

Frank

Noted!  I can another dome on the bottm.  Do you think applying a small ring of some sort of foam, for the domes to sit on, would be a bad idea?
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Offline ManateeMafia

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Re: KX Reference
« Reply #7 on: May 14, 2017, 08:23:00 pm »
With that glass dome it reminds me of Gallifrey. If you are a Dr. Who fan then even better. Of course that would be more of a reference for a time-nut.
 

Offline mimmus78

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Re: KX Reference
« Reply #8 on: May 15, 2017, 12:14:24 am »
Isn't the dome too big and too far away to prevent air drafts?

My guts tell me the dome must be near the ltz1000 ... the less air there is, the less gradient there is, the less drafts there be.

But I maybe completely wrong there.

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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #9 on: May 15, 2017, 02:03:13 am »
Isn't the dome too big and too far away to prevent air drafts?

My guts tell me the dome must be near the ltz1000 ... the less air there is, the less gradient there is, the less drafts there be.

But I maybe completely wrong there.

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I would think the dome would cause the air inside to be stagnant, right?  And just sit there, slowly reaching equilibrium with the air outside of it?  I could very well be wrong though.


With that glass dome it reminds me of Gallifrey. If you are a Dr. Who fan then even better. Of course that would be more of a reference for a time-nut.

I tried but couldn't really get into it.  The idea came to me while reading through the LTZ1000 thread.
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Online Vgkid

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Re: KX Reference
« Reply #10 on: May 15, 2017, 03:01:17 am »
I would think the dome would cause the air inside to be stagnant, right?  And just sit there, slowly reaching equilibrium with the air outside of it?  I could very well be wrong though.
I was thinking the same. It is only about 2cm^3, so not much volume. I would also assume that the ltz package would take up most of that.
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Offline IconicPCB

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Re: KX Reference
« Reply #11 on: May 15, 2017, 04:58:46 am »
Doctor Who is OK when viewed purely as a bit of sci fi.
But then so is Startrek...
HOWEVER... neither can be ignored on basis of their contribution to social and political commentry.
 

Offline mimmus78

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Re: KX Reference
« Reply #12 on: May 15, 2017, 10:20:33 am »
>> I would think the dome would cause the air inside to be stagnant, right?
>> And just sit there, slowly reaching equilibrium with the air outside of it?

Well maybe this is good experiment to do with the low noise amplifier and
check if there is differences ... actually I'm a lot busy and than I don't have
the dome.
 

Online Kleinstein

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Re: KX Reference
« Reply #13 on: May 15, 2017, 03:16:30 pm »
The question with the size of the air space above the reference is, if this is large enough to develop a significant  convection flow, especially if it even turns turbulent. So 2 cm² might be just acceptable, but a little less might be better.

With the wire would resistors, I would definitely use a different layout made for the larger form factor: Bending the wires so much to fit them to the KX board can ruin the stability and if mounted vertically, it can cause thermal EMF problems. The other point to change in that step would be to go back to the more suitable LT1013 instead of 2 single OPs. AZ OPs here can cause more trouble than good. Similar to the drift of the resistors, offset drift of the OPs is attenuated by a factor of about 200.
 
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #14 on: May 15, 2017, 05:37:59 pm »
The question with the size of the air space above the reference is, if this is large enough to develop a significant  convection flow, especially if it even turns turbulent. So 2 cm² might be just acceptable, but a little less might be better.

With the wire would resistors, I would definitely use a different layout made for the larger form factor: Bending the wires so much to fit them to the KX board can ruin the stability and if mounted vertically, it can cause thermal EMF problems. The other point to change in that step would be to go back to the more suitable LT1013 instead of 2 single OPs. AZ OPs here can cause more trouble than good. Similar to the drift of the resistors, offset drift of the OPs is attenuated by a factor of about 200.

I'll see if I can get some smaller glass domes for relatively cheap.

And I agree, with my own design I will be doing, I plan on using the LT1013A.  I'll be sure to design enough room for bulky WW resistors when I get to laying a board out.
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Offline mimmus78

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Re: KX Reference
« Reply #15 on: May 15, 2017, 09:28:10 pm »
I used insulating foam (the one used in walls). It's more dense than standard padding foam and very easy to "machine/cut" with a sharp knife. I think it's also not so much flameable ...

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Offline Zucca

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Re: KX Reference
« Reply #16 on: May 18, 2017, 11:42:51 am »
Next Chapter: Vacuum Chamber for the ltz package  >:D

Maybe a PVC Block with an air valve screwed on it and seal with a O Ring?

some inspirations...just writing without thinking too much... in this boring work day..

http://heater.belilove.com/article_192_Circuit-Board-Mounted.cfm
« Last Edit: May 18, 2017, 11:48:22 am by zucca »
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Offline kj7e

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Re: KX Reference
« Reply #17 on: May 18, 2017, 12:57:50 pm »
I keep thinking, why not just place the entire board in an enclosed, thermally stable temperature regulated box?  So all of the components are  at a constant temp.
 

Offline Conrad Hoffman

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Re: KX Reference
« Reply #18 on: May 18, 2017, 01:22:03 pm »
I can't think of anything good about putting the board in a vacuum chamber. Better to fill the chamber with dry nitrogen or argon, or immerse everything in an oil bath.
 

Offline tggzzz

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Re: KX Reference
« Reply #19 on: May 18, 2017, 01:29:00 pm »
I keep thinking, why not just place the entire board in an enclosed, thermally stable temperature regulated box?  So all of the components are  at a constant temp.

Some do just that, e.g. my vintage Trancell-II. https://www.eevblog.com/forum/metrology/standard-reference-labs-trancells-any-information-available/

That has a zener in a temperature-controlled box, plus a mains supply in a different box, plus gel-cells so it isn't reliant on the mains supply - all thermally insulated in an instrument case the size of an Agilent DMM.
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #20 on: May 18, 2017, 02:18:04 pm »
I keep thinking, why not just place the entire board in an enclosed, thermally stable temperature regulated box?  So all of the components are  at a constant temp.

This is what I will be doing in my own personal design. 
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Offline Conrad Hoffman

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Re: KX Reference
« Reply #21 on: May 18, 2017, 03:24:40 pm »
CalM, a friendly request- I love pictures of boards, parts and teardowns, but if you could downsize these slightly it would greatly help my steam-powered antique computer and economy 'net connection. All my money goes into test equipment and health care! Here's a 4 meg image downsized to under 350 k. Quality loss is, I think, minimal.

 
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #22 on: May 18, 2017, 03:28:43 pm »
CalM, a friendly request- I love pictures of boards, parts and teardowns, but if you could downsize these slightly it would greatly help my steam-powered antique computer and economy 'net connection. All my money goes into test equipment and health care! Here's a 4 meg image downsized to under 350 k. Quality loss is, I think, minimal.

Yes!  I will see what I can do here, soon.   I apologize for the massive pictures
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Offline babysitter

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Re: KX Reference
« Reply #23 on: May 18, 2017, 05:56:54 pm »
It needs more JPEG! :-DD
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Offline PedroDaGr8

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Re: KX Reference
« Reply #24 on: May 18, 2017, 11:49:12 pm »


Here you go.
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Offline feedback.loop

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Re: KX Reference
« Reply #25 on: May 20, 2017, 06:25:08 am »
This is my build of the KX reference. Overall the project went very well. The reference worked on the first attempt. The output voltage was monitored for about 46 hours so far using HP 34401A and Datron 1071. The graphs look great overall, but with some small unexplained glitches.

https://youtu.be/mgHhGDRKZjo
 
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Offline branadic

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Re: KX Reference
« Reply #26 on: May 20, 2017, 09:14:59 am »
Would you mind plotting voltage (y-axis) over temperature (x-axis)? This way you can better see dependency.
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Offline Dr. Frank

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Re: KX Reference
« Reply #27 on: May 20, 2017, 10:08:21 am »
Both DMMs are much more noisy and less stable (about 10 times) than the LTZ1000 circuit.

The 34401As internal LM399 may produce these 1..2ppm steps.

The bigger glitches may be produced by the LTZ1000 circuit, caused by RF disturbances, from switch mode power supplies in your lab. Watch out for LED lighting..
xdevs circuit lacks additional capacitors, which suppress most of these disturbances. I added 2 capacitors to the LT circuit, and things improved a lot, already.
Such glitches vanished completely, for my circuits.

So please consult the Super LTZ1000 thread for details on Andreas' circuit.

Also, you might trim the circuit for smallest T.C.
For that, you would need a 2nd LTZ circuit at constant temperature.
Frank
 
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Offline SvanGool

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Re: KX Reference
« Reply #28 on: May 20, 2017, 10:49:08 am »
To save time on scanning through 80 pages of the "Super LTZ1000" thread, I think Dr. Frank is referring to Andreas' explanation on removing distortions and his overall explanation of his circuit.
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Offline feedback.loop

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Re: KX Reference
« Reply #29 on: May 22, 2017, 11:35:42 pm »
Would you mind plotting voltage (y-axis) over temperature (x-axis)? This way you can better see dependency.

Here is the plot.
 
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #30 on: May 24, 2017, 12:25:28 am »
Both of my KX references are up and cooking!  I currently only have 1 meter at home, so in about a week ill start logging some data on one of the references to share!   :scared:
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Offline Ordinaryman1971

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Re: KX Reference
« Reply #31 on: May 24, 2017, 06:24:19 pm »
Is there somebody making more of those boards? I would be interested in building one myself and even more in making few of the low cost LM399 ones. TiN, do you have some spares please :)
 

Offline kj7e

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Re: KX Reference
« Reply #32 on: May 27, 2017, 06:06:08 am »
Both of my KX references are up and cooking!  I currently only have 1 meter at home, so in about a week ill start logging some data on one of the references to share!   :scared:

Got all of my parts ordered today.
 

Offline TiN

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Re: KX Reference
« Reply #33 on: June 05, 2017, 05:41:25 pm »
As I received fresh LTZ chips from LTC, time to get them installed and start logging. I've used my two last KX boards as test venicles here.
Both PCBs unlike rest of the references have AUGAT socket, and LTZ chips installed without soldering, with trimmed legs. (1 x CH and 1 x ACH).

PCBs bit different too, one is from Sjef, latest version B03, and one of my own older ones B01 with few patches. Detailed config:

* SvanGool's purple KX B03 PCB, 2xLTC2057, Edwin PWW 12.5K+1K bodged & crooked, VHP202Z 120?, 75K? <1ppm/K PTF56 x 2. LTZ1000A 2017 chip in AUGAT socket.

* xDevs.com B01 PCB, 2xLTC2057, few extra caps per Andreas schematics, AE 15K+100K, S102 174+312R, AE 50K+30K, AE 50K+30K, AE 1K foil resistors, LTZ1000CH 2016 49week chip in AUGAT socket, 390K compensation resistor present.



Few more photos of board.




Initial datalog started, ppm levels are reset for new references:

Code: [Select]
Channel 1: VM1=7.072588550, VM2=7.072588602, AVG = 7.072588576, -0.2825 ppm
Channel 2: VM1=7.129833446, VM2=7.129833183, AVG = 7.129833314, 0.3918 ppm
Channel 3: VM1=7.136680531, VM2=7.136680303, AVG = 7.136680417, 0.1275 ppm
Channel 4: VM1=7.184637357, VM2=7.184637357, AVG = 7.184637357, 0.8055 ppm
Channel 5: VM1=7.129231640, VM2=7.129231482, AVG = 7.129231561, 0.3414 ppm
Channel 6: VM1=7.136664333, VM2=7.136664053, AVG = 7.136664193, -0.2630 ppm
Channel 7: VM1=7.128692837, VM2=7.128692784, AVG = 7.128692811, -0.5456 ppm
Channel 8: VM1=7.134149909, VM2=7.134149594, AVG = 7.134149751, -0.3853 ppm

Channel 1: VM1=7.072587902, VM2=7.072587989, AVG = 7.072587946, -0.3716 ppm
Channel 2: VM1=7.129833831, VM2=7.129833901, AVG = 7.129833866, 0.4692 ppm
Channel 3: VM1=7.136680426, VM2=7.136680478, AVG = 7.136680452, 0.1324 ppm
Channel 4: VM1=7.184636866, VM2=7.184637094, AVG = 7.184636980, 0.7530 ppm
Channel 5: VM1=7.129231534, VM2=7.129231377, AVG = 7.129231455, 0.3266 ppm
Channel 6: VM1=7.136664018, VM2=7.136663948, AVG = 7.136663983, -0.2924 ppm
Channel 7: VM1=7.128692346, VM2=7.128692136, AVG = 7.128692241, -0.6255 ppm
Channel 8: VM1=7.134150031, VM2=7.134150137, AVG = 7.134150084, -0.3387 ppm

Channel 8 is VK5RC's ref externally from the chassis. All powered from linear +15V LDO supply, scanned thru Keithley 7168 + RPI and sampled by 3458A NPLC100.

Now I don't have any more LTZ references left, time to move on to other projects related  ^-^.
Will be interesting to compare drift of my older references (which are 24/7 for few months already) to this two brand new fresh ones.  :-DMM
« Last Edit: June 05, 2017, 05:51:24 pm by TiN »
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Offline Conrad Hoffman

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Re: KX Reference
« Reply #34 on: June 05, 2017, 05:52:09 pm »
Is there somebody making more of those boards? I would be interested in building one myself and even more in making few of the low cost LM399 ones. TiN, do you have some spares please :)

Me too!
 

Offline hwj-d

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Re: KX Reference
« Reply #35 on: June 05, 2017, 05:59:29 pm »
@TiN, thanks a lot, but
please give me a tip, from where i can get these pcb's one for lm399 and one KX? 
 

Offline Muxr

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Re: KX Reference
« Reply #36 on: June 05, 2017, 06:21:03 pm »
There is a project on OshPark that lets you order (3 is the smallest run). https://oshpark.com/shared_projects/HfKcqjV3

Dunno if anyone has any spares.
 
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Offline kj7e

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Re: KX Reference
« Reply #37 on: June 05, 2017, 08:50:34 pm »
I have three LTZ1000 purple KX B03 PCB boards on order, I should only need one provided I don't mess it up.  So I should have two available if someone wants.  Send me a PM.
« Last Edit: June 05, 2017, 09:15:09 pm by kj7e »
 
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Offline hwj-d

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Re: KX Reference
« Reply #38 on: June 05, 2017, 10:31:54 pm »
@kj7e
send PM
 

Offline RandallMcRee

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Re: KX Reference
« Reply #39 on: June 05, 2017, 11:01:05 pm »

Three more on order from me, as well! I think will keep two so if anyone wants one, ping me.

Did not see this thread before ordering mine from OSH!

Should have a few more LTZ1000s in the US Cal Club. Exciting. I have to confess I am going to try and go cheaply (TE Connectivity 15 ppm) on the resistors and put them in an oven, which I already constructed. See how that compares to the much more expensive Vishay/Pettis builds.

Randall.
 

Offline ManateeMafia

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Re: KX Reference
« Reply #40 on: June 06, 2017, 01:44:55 am »
LT has been good to me too. I received an order last week from them. My board will be more of the traditional, boring, thru-hole design.

 
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Offline RandallMcRee

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Re: KX Reference
« Reply #41 on: June 06, 2017, 03:33:21 am »
Why 5? Seems like an interesting number...tell us more.

 

Offline ManateeMafia

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Re: KX Reference
« Reply #42 on: June 06, 2017, 03:46:51 am »
My first rev will be one or two populated boards. Once I feel comfortable with the component choices and fix my initial errors, I will get the second improved batch made.

The first rev pcb has a header for a piggy-back board that will allow me to try different buffer amps and 10v boost designs without building several LTZ boards. Once I settle on something, the next rev will have that design added to it and I can build 3 more for long term testing. I have a Data Proof scanner I plan on using for long term data collection.

 
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Offline TiN

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Re: KX Reference
« Reply #43 on: June 06, 2017, 04:40:14 am »
ManateeMafia
Sounds like somebody was working :) Looking forward for the data.
What resistors and temperature setpoints are you going to use?

Meanwhile, first 12 hours of data :



Note remind: Whole setup was cold, powered off for 2 days. Now added two fresh LTZ chips (Channel 5 is LTZ1000A and Channel 7 is LTZ1000).
First two hours it took to warm up and stabilize with ~1ppm change on all of references.

Channel 1 is good old jumper LTZ1000A from eBay :). It's stable, just jumpy. Good for ADC resolution testing, I bet, as jumps are fairly constant level ~0.7ppm.
Channel 2 is non-modified HP 3458A A9 reference module, rest are my KX boards.

P.S. ambient is about 25C, reading has correction +2.0c due to proximity of BME280 to FPGA board.
« Last Edit: June 06, 2017, 04:42:16 am by TiN »
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Offline MK

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Re: KX Reference
« Reply #44 on: June 06, 2017, 11:04:30 am »
Perhaps you could try running channel1 jumper LTZ at a higher current to see if that makes the jumps go away? Something for a rainy day when you feel you have enough history and they all seem to have stabilised.
 

Offline d-smes

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Re: KX Reference
« Reply #45 on: June 06, 2017, 11:30:34 am »
@TiN-  What's the slight step down at 6:30?  Did the sun rise and shine on your test leads?  ;)  Even your eBay jumper follows along...
 

Offline SvanGool

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Re: KX Reference
« Reply #46 on: June 06, 2017, 12:52:12 pm »
@TiN

Thanks for sharing !

Can you detail a bit more which reference is on which channel?

My gamble:
Ch1: "Good old jumper"
Ch2: HP 3458A A9 reference module
Ch3: VK5RC KX Reference
CH4: B03 reference
CH5: B01 reference with Andreas' capacitors
......

Andreas added following components with reference to your VREF_B02 schematic, to improve the noise and stability of the standard design:
  • 100 nF between U1-6 and GND (lower noise)
  • 100 nF between U1-4 and GND (lower noise)
  • 100 nF between U6-2 and U6-3 (lower RF noise)
  • 100 nF between U5-2 and U5-3 (lower RF noise)
  • 100 nF between U5-6 and GND + 10K between U5-5 and U1-4  (improve loop stability)
  • 100 nF between VREF+ and VREF- at the output connector (block RF from output)
Andreas could only do item 6 when item 5 was implemented, with the opamp he used (LT1013), which, when needed, would probably require some PCB-trace/guard changes on the KX-board.

You mentioned you implemented some of Andreas' suggestions, what did you add on the B01 board of above items ?  >:D
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Offline kj7e

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Re: KX Reference
« Reply #47 on: June 10, 2017, 04:01:47 pm »
Maybe a B04 version with some of the filtering in the future?

Working on my B03 board now.



Going to use 13K/1K on the heater with the LTZ1000A.  Also going to buffer the output with the LTC1150/LT1010 combo and place in side an heated (35 deg C) die cast box.  Plan is to build it all in a nice battery powered chassis.  But one step at a time.

 
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Online Kleinstein

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Re: KX Reference
« Reply #48 on: June 10, 2017, 04:26:20 pm »
Filtering likely only makes sense with an additional buffer. It would reduce higher frequency noise only, which is not a big deal in many application (e.g. reading with an DMM) anyway. But of cause if a buffer is build, one could include at least some filtering, if this is not adding too much DC errors and additional low frequency noise.

In this case a just an AZ OP (also with an additional power stage) might not be the best choice as a buffer, since this could easily add again some higher frequency noise (though usually different frequency band). To really make full use of a filter, it would need some a low noise and background one (e.g. compound with the AZ Op only for the LF part).
 
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Offline kj7e

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Re: KX Reference
« Reply #49 on: June 10, 2017, 09:00:05 pm »
It will be a few weeks (maybe months) before the Vishay parts are in, but I wanted to get it fired up and let it burn in until then.  Who needs precision resistors anyway?

Instantly, like with in 2 seconds it was reading 7.1330703 and its not moved.   :-+








I also decided to space the LTZ1000A above the board slightly.  Since I will be placing the reference and buffer boards in a thermally stable box, this only made sense to me;


Edit, LTC1150/LT1010 buffer working on the bread board.;

« Last Edit: June 11, 2017, 02:57:29 am by kj7e »
 

Offline kj7e

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Re: KX Reference
« Reply #50 on: June 11, 2017, 02:49:46 am »
Sorry for all the photos Conrad  ;D

Had some closed cell hi-temp foam laying around so made top hat, reduced the heater current draw by almost 1mA while out in the open with moving air in the shop.









Edit, I found air moving under the LTZ1000A had just as much effect as directly on the metal can.  So slight modification to the foam hat.  Enlarged the hole for the can so there is no direct contact and made it taller to come all the way to the board.  This very effectively stabilizes the effects of air turbulence.  Originally I wanted to keep the foam off the board and traces.  Think I may use some silicon to tack it to the board. 

Made a short video showing the effects before and after;
https://youtu.be/sYhQBudCLiU
« Last Edit: June 11, 2017, 05:28:18 pm by kj7e »
 

Offline Andreas

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Re: KX Reference
« Reply #51 on: June 11, 2017, 05:34:18 pm »
Hello,

do not forget to (air-)shield the pins from the other side of the PCB.

with best regards

Andreas
 
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Offline rigrunner

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Re: KX Reference
« Reply #52 on: June 12, 2017, 10:55:46 pm »
@TiN, thanks a lot, but
please give me a tip, from where i can get these pcb's one for lm399 and one KX?

Prompted by Svangool's LTZ project upload, and with help from the guys at OSHPark for the drill file conversion, i've uploaded a shared project for TiNs LM399 KX-ref PCB Version S02 here: https://oshpark.com/shared_projects/oaEZl86b (with TiNs permission).

As per Svangool's project the minimum order at OSH Park is three boards, these cost in total $49.80 ($16.60 per board), including standard international shipping, excluding any import taxes or other costs.

These are as yet untested.

RR
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Offline Muxr

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Re: KX Reference
« Reply #53 on: June 18, 2017, 04:39:11 pm »
Has anyone had luck running the KX reference using the 100K values for the original? 70K   (R6,R7). I thought I saw somewhere that this is a viable substitution. I got all the other resistors but 70K is hard to find.

I would like to substitute them with this resistor: http://www.mouser.com/Search/ProductDetail.aspx?R=Y0062100K000T9Lvirtualkey59450000virtualkey71-S102KT100K00TB
 

Offline hwj-d

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Re: KX Reference
« Reply #54 on: June 18, 2017, 07:37:35 pm »
I will try 80k, 2x2 of them:
http://www.ebay.com/itm/110983067006

They and other parts+pcb's are on the way. So, assembly will be next month so far.
 

Offline 0.01C

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Re: KX Reference
« Reply #55 on: June 18, 2017, 08:10:05 pm »
I will try 80k, 2x2 of them:
http://www.ebay.com/itm/110983067006

They and other parts+pcb's are on the way. So, assembly will be next month so far.

try
https://world.taobao.com/item/521116800640.htm?spm=a312a.7700714.0.0.2LAU7Z#detail
0.01℃
 

Offline Alex Nikitin

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Re: KX Reference
« Reply #56 on: June 18, 2017, 10:16:32 pm »
Hmm, I'm not sure if it is OK from the forum rules POW  :-// , I have a number of Vishay S102C 87.15K 0.01% resistors, about 18 years old, still very accurate. That is what I plan to use for my own LTZ1000 boards in place of 70K resistors, however I can sell some of these for LTZ reference use and much cheaper than prices on Digikey/Mouser/etc. for S102 types. PM me if it is of interest.

Cheers

Alex
« Last Edit: June 18, 2017, 10:51:20 pm by Alex Nikitin »
 

Offline kj7e

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Re: KX Reference
« Reply #57 on: June 19, 2017, 12:07:02 am »
Been working with a Die Cast aluminum Bud Box where the KX reference and buffer/follower boards will reside.  Decided to ovenize it, set at a reasonable 35 deg C (one of the reasons I decided on using higher temp 13K for the heater).  The oven control circuit is working very well, and seems to hold the internal air temp to well within 0.1 deg C.  Still playing with the feedback gain and placement of the thermister for best performance, its a very slow process.  Meanwhile the KX board cooks away with 1 cent metal film resistors and has not budged, Ill have a 1000 hours on the can by the time the Vishay parts arrive.  My plan is to build everything in a small portable enclosure with 10AH of battery power.  Photos and test results to come.

Used some closet shelf angle brackets to make a nice mount for the KX board;


Initial testing to see how much power would be needed to heat the box;


Decided on 2x 25 Ohm 10 watt resistors in series for a 50 Ohm heater load;


This will heat the box from 20 deg C to 35 deg C in about 20 min with 20 volts at 0.4 amps (8 watts)


Playing with the feedback gain;


Still very much in proto stage, but its coming along nicely;


Edit, some temp ramp and stability graphs;

From 20 deg C its within half a deg of 35 in about 30 min.


Zoomed in, 0.5 deg FS, it holds within 0.1 dec C.  I'm at the limits of my temp measuring ability, not sure I can tune anymore ripple out, but I'm happy with this.
« Last Edit: June 20, 2017, 12:05:07 am by kj7e »
 
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Offline kj7e

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Re: KX Reference
« Reply #58 on: June 25, 2017, 04:28:59 am »
Building the portable battery powered enclosure;









After final placement of the 10K NTC sensor in the oven and a second layer of foam insulation temp stability is far below +/- 0.1C.  even better than +/- 0.05C best I can tell.  I'm now using a second precision 10K NTC sensor and my 34465a 4W to measure the air temp inside the oven, this seems to be far mare accurate than the K type thermocouple .  The sensor at 35 Dec C is 6,531.0 Ohm and 270.5 Ohm/Dec C at this point.  So 27.05 Ohm/0.1 Dec C, with the trend chart 27 Ohm FS, the line is nearly flat.



Warm up plot from 25 Deg C to 35 Deg C;


Full scale is 0.1 Deg C;


Edit, final oven control circuit attached.
« Last Edit: April 17, 2018, 07:16:21 pm by kj7e »
 
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Offline cellularmitosis

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Re: KX Reference
« Reply #59 on: June 25, 2017, 05:41:33 am »
Very cool!  Er, I mean warm!  Duh, nice work!
LTZs: KX FX MX CX PX Frank A9 QX
 

Offline rigrunner

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Re: KX Reference
« Reply #60 on: June 29, 2017, 06:07:36 pm »
I was planning on ovenizing my LTZ boards.  Just waiting on parts to finish off the second build.
Why did you choose to mount the resistors outboard of the enclosure kj7e?

The OSH lm399 boards have arrived.

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Offline RandallMcRee

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Re: KX Reference
« Reply #61 on: June 29, 2017, 07:04:08 pm »
Question for the LTZ1000 experts.

I am putting together a new KX reference board.

I have some LTC5400 resistor packs which I am planning on using for R4/R5. On hand are the "LT5400-8 1k 9k    1:9" and    "LT5400-3 10k 100k 1:10". Looking for a nominal 1:12 ratio.

The -8 with suitable parallel series combos gives a ratio of 900 ohms/10000 ohms.
The -3 gives a better fit to 1:12 with 9090/110000 ohms.

Is it a concern that the -3 absolute values are 10 times higher than the data sheet spec?
 

Offline kj7e

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Re: KX Reference
« Reply #62 on: June 29, 2017, 07:07:00 pm »
The heater resistors?  Two main reasons, easier to wire, less erroneous energy/possibility of noise within the shielded housing.

Made some progress on the overall enclosure;






Still need to mount the pair of 5s 5000mAh Li-Po's and build the input power switching circuit (auto switch to external power if over 18v in).  Once the Vishay resistors come in Ill finish the KX board and mount it in the oven.  After a month of running it reads just a few uv below where it did when I first powered it on, and that's with cheap 1/4 watt resistors.
« Last Edit: June 29, 2017, 07:09:19 pm by kj7e »
 

Online Kleinstein

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Re: KX Reference
« Reply #63 on: June 29, 2017, 07:21:38 pm »
A much higher absolute value for the divider is a problem. There is some base current flowing through the divider and this current can change with aging. Often also 100 K resistors are less accurate, as this is in a range where leakage starts to get important.

The ratio of 1:12 is still a rather low temperature.
 
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Offline RandallMcRee

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Re: KX Reference
« Reply #64 on: June 29, 2017, 10:35:24 pm »
Is there a formula that determines the oven temperature given R4, R5?

I've read extensively but not seen it...

Thanks!
 

Offline cellularmitosis

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Re: KX Reference
« Reply #65 on: July 02, 2017, 03:49:21 am »
Is there a formula that determines the oven temperature given R4, R5?

I've read extensively but not seen it...

Thanks!

I haven't read through every page of the LTZ thread yet, but I did find this: https://www.eevblog.com/forum/metrology/ultra-precision-reference-ltz1000/msg380638/#msg380638

Quote from: Galazyrise
From that, I determine that T = 310 - 7*500*R5/(R4+R5)

Here's a table from my notes:

Note: I do recall reading somewhere that the formula isn't exact: there could be up to a 5 degree offset from the formula due to manufacturing variations.  Don't quote me on that though.
« Last Edit: July 02, 2017, 03:51:16 am by cellularmitosis »
LTZs: KX FX MX CX PX Frank A9 QX
 
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Offline Muxr

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Re: KX Reference
« Reply #66 on: July 04, 2017, 01:40:26 am »
The right resistors finally arrived. I put my KX in one of those mini Pelican cases, nothing special:



The heat shrink tubing is hiding a protection diode and some ferrite beads. The waiting (burn in), begins.
 
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Offline Muxr

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Re: KX Reference
« Reply #67 on: July 07, 2017, 03:31:42 pm »
I am pretty impressed with what I am seeing so far in terms of TC and noise. This is compared to my best reference, Doug Malone's 10V LT1021 (battery powered). LTZ1000 KX is powered of a lab power supply. Built from scrounged up foil resistors from Ebay/China, and no doubt still has a lot of hysteresis to burn through. It's only been on for a few days, since the soldering iron touched it.





I have enough resistors to build a second one. Any advantage to going with a LTZ1000ACH version for the 2nd one?

edit:
Battery powered and semi shielded by a tin box:
« Last Edit: July 08, 2017, 11:27:35 pm by Muxr »
 
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Offline TiN

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Re: KX Reference
« Reply #68 on: July 07, 2017, 04:12:34 pm »
Try without aircon, as those oscillations aren't helpful :). If I'm reading your graph correctly, you see 1.6ppm pk-pk? That's bit much, I usually get around 0.5-0.6ppm pk-pk for week long captures, or 0.3-0.4ppm pk-pk daily. Example here and here, with K7168 switch scanner in place.

Before fellow voltnuts here start blaming chopper opamps, CH2 reference on my graphs is "proper" HP 3458A A9 for comparison reasons :).

Also if you measure ref like it's shown on photo - add foam cap on top and bottom of the zener, even when it's inside the box. That tame drafts even in still air a bit.

As for ACH version, if you want to try - sure, why not, but unless you running on battery, you wouldn't be able to separate data result from either CH or ACH.
« Last Edit: July 07, 2017, 04:17:50 pm by TiN »
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Offline MisterDiodes

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Re: KX Reference
« Reply #69 on: July 07, 2017, 04:19:22 pm »
Muxr: Use the "A" version.  The non A requires that extra TC compensation resistor and in 5-10 yrs time that will need a re-trim for best performance - otherwise it can add more trouble than it solves in the future.  That's the whole point of the "A" version (it doesn't need the extra resistor), and that's why it was developed for 3458a.   

Randall:  LTC5400 diffused resistor packs don't have a lot of use around LTZ circuits.  Suggest you just get some PWW made from Pettis or GR or Rhopoint, etc.  Those will give you better performance for a cheaper price.  You don't want a 12:1 ratio either.  If this is your first unit stick with 13k/1k as datasheet tells you or if you know it'll never get warm maybe 12.5k over 1k.  Plenty of decades 3458a's don't drift 1ppm /yr with their standard 15k / 1k, and learn from that. 

You select your heater resistor ratio for your enclosure and application.  You don't want the die too hot, but it has to have a setpoint warm enough that the heater circuit can control the temperature.  You know if it's too cold when the ambient temp rises and you see the LTZ lose control of the die temperature, and that is pretty obvious.  You do this by testing.  There are charts out there but not very accurate because each die is different.  Watch your Del-Vbe of the heater sense transistor to see what the die temp is on -your- setup at your ambient temp.

The problem with the assumption that warmer temps will cause the die to drift faster was made by people not really understanding the underlying mechanism that causes drift in the substrate crystal lattice in the first place.  If you have a -very- stable die to begin with, it's going to run warmer in a very stable condition also.  If you happen to get a die that has a higher internal strain, yes the higher temp will cause a somewhat faster drift rate initially...BUT a lot of times what happens is those higher strain die begins to assume a more relaxed state - and in say 10 ~ 12 years they will settle down and become very good performers as the crystal strain-relieves itself, atom by atom.  This is not an experiment for impatient people, but you do learn what the reality is after a while.

Again, the time frame you're looking at for initial break in is on the order of months, and then you look at the first 5~8 years for initial performance, and then start looking at the 10~25~30 year performance and you see a bit different story as the die really settles into it's final state.

You don't have to believe me, ask any 30yr old 3458a that goes in for cal and hasn't moved except maybe 1ppm or less per year.  And has been doing that for the last 10 years or so.  Not all do that of course but a lot do...and they all run 15k over 1k for the heater resistor ratio, because it's warm inside that box.
« Last Edit: July 07, 2017, 04:31:37 pm by MisterDiodes »
 
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Offline Muxr

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Re: KX Reference
« Reply #70 on: July 07, 2017, 04:20:38 pm »
Try without aircon, as those oscillations aren't helpful :). If I'm reading your graph correctly, you see 1.6ppm pk-pk? That's bit much, I usually get around 0.5-0.6ppm pk-pk for week long captures, or 0.3-0.4ppm pk-pk daily. Example here and here, with K7168 switch scanner in place.

Before fellow voltnuts here start blaming chopper opamps, CH2 reference on my graphs is "proper" HP 3458A A9 for comparison reasons :).
No way can I live without aircon (Summer in Florida) but fret not Tin.. I am building a micro environmental chamber, so I should be able to get readings from a much more controlled environment. (although can't put my hp3458a into it) ;) In winter I can do measurements without aircon.

I am still very impressed with the results, usually my results are in 5ppm p-p range or more under my usual lab conditions, lots of airflow and aircon activity as you noticed.
 

Offline Muxr

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Re: KX Reference
« Reply #71 on: July 07, 2017, 05:58:07 pm »
@MisterDiodes

Thanks for the info.. will try the LTZ1000ACH next. The heater setpoint I am using is 1K - 12K7 closest I have in Vishay foil variety. I need to checkout some of these other sources of low TC resistors you outlined.
 

Offline RandallMcRee

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Re: KX Reference
« Reply #72 on: July 08, 2017, 03:17:21 am »
Quote
Randall:  LTC5400 diffused resistor packs don't have a lot of use around LTZ circuits.  Suggest you just get some PWW made from Pettis or GR or Rhopoint, etc.  Those will give you better performance for a cheaper price.  You don't want a 12:1 ratio either.  If this is your first unit stick with 13k/1k as datasheet tells you or if you know it'll never get warm maybe 12.5k over 1k.  Plenty of decades 3458a's don't drift 1ppm /yr with their standard 15k / 1k, and learn from that. 

I took your advice, above, and tore out my ltc5400 and replaced it with two TE Conn 15ppm resistors with a 1:12.5 ratio (these were on hand). Previously, it was exhibiting strange drifting. Gone. Very stable at least for the the first five hours.

Thanks again.
 

Offline MisterDiodes

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Re: KX Reference
« Reply #73 on: July 08, 2017, 08:34:05 pm »
Quote
Randall:  LTC5400 diffused resistor packs don't have a lot of use around LTZ circuits.  Suggest you just get some PWW made from Pettis or GR or Rhopoint, etc.  Those will give you better performance for a cheaper price.  You don't want a 12:1 ratio either.  If this is your first unit stick with 13k/1k as datasheet tells you or if you know it'll never get warm maybe 12.5k over 1k.  Plenty of decades 3458a's don't drift 1ppm /yr with their standard 15k / 1k, and learn from that. 

I took your advice, above, and tore out my ltc5400 and replaced it with two TE Conn 15ppm resistors with a 1:12.5 ratio (these were on hand). Previously, it was exhibiting strange drifting. Gone. Very stable at least for the the first five hours.

Thanks again.

You might have been running just a little too cold, but glad it's working now!!
 

Offline Muxr

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Re: KX Reference
« Reply #74 on: July 08, 2017, 11:55:26 pm »
@TiN

I've updated the post https://www.eevblog.com/forum/metrology/kx-reference/msg1250845/#msg1250845

With a short run powering the reference from a 12V battery. I am getting 0.6ppm peak to peak with that setup. I suspect I can further improve the performance by improving my cable / probe situation (I am just using the tiny micro test clips with a twisted pair which are not the best).

In either case, that standard deviation is an order of magnitude better than I've seen from any other reference I have.

 

Offline TiN

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Re: KX Reference
« Reply #75 on: July 09, 2017, 12:09:57 am »
Looking better now. Should be no much difference running from battery or DC supply, if all grounding done right.
I'd avoid any kind of clips or connectors between the reference and meter and use freshly cut copper twister pair (CAT5e/6e lan cable works best for that, with shield connected only one side, at DMM guard LO).
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Offline Muxr

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Re: KX Reference
« Reply #76 on: July 09, 2017, 06:18:43 pm »
Was about to order a LTZ1000A.. digikey is out of stock, ordered it directly from LT but I also got a warning that it will likely take a while. Which one of you bought up all the LTZ1000As?  ;)

TME in europe has them but they are a bit more expensive. Will just wait until LT ships me mine.
 

Offline TiN

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Re: KX Reference
« Reply #77 on: July 09, 2017, 07:00:00 pm »
That warning is there as long as I remember, but never was a problem for few pcs qty I was ordering before.
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Offline kj7e

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Re: KX Reference
« Reply #78 on: July 11, 2017, 08:41:51 pm »
Quick update on my KX portable battery powered ovenized enclosure.  Everything fits and works, just waiting on the Vishay resistors before I can complete the buffer.

https://youtu.be/OuonZGQq0Q4

 
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Offline TiN

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Re: KX Reference
« Reply #79 on: July 11, 2017, 08:50:34 pm »
I like it. What is the case model? It seems perfect size for such kind of project. Next step to put some Raspberry Pi inside for datastorage/logging and external meter control, so you can always keep digital history of the reference together with the box, making it perfect travel standard.
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Offline kj7e

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Re: KX Reference
« Reply #80 on: July 11, 2017, 09:01:11 pm »
I like it. What is the case model? It seems perfect size for such kind of project. Next step to put some Raspberry Pi inside for datastorage/logging and external meter control, so you can always keep digital history of the reference together with the box, making it perfect travel standard.

Bud Industries TR-6100;
http://www.budind.com/view/Small+Metal+Electronics+Enclosures/TR+Series+Small+Cabinet

If you search around you they can be found at a discount.  The Die Cast box used for the oven/shielding is a Bud Industries CU-4234.  The Raspberry Pi with environmental logging is a good idea, maybe for V2.  Once this one is built, I hope to send it off to someone with a freshly calibrated 3458A or better to measure/adjust.
 
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Offline lukier

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Re: KX Reference
« Reply #81 on: July 11, 2017, 09:12:49 pm »
kj7e: nice build. Thanks for the info on the case. What are you planning for the output protection (short circuit, feeding in voltage, maybe gas discharge tube)?
 

Offline Edwin G. Pettis

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Re: KX Reference
« Reply #82 on: July 11, 2017, 09:38:41 pm »
The Bud case is very nice and very well made, also expensive.  I used a TR6102 for my winding machine controller and the last time I checked they had jumped to $225.00 (about $100 higher than they used to be).  Yipes, I just checked latest pricing and they're up to $275.00, ridiculous.  I did find a 'discounted' price of $244 at one place, still pricey.
 

Offline kj7e

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Re: KX Reference
« Reply #83 on: July 11, 2017, 10:58:31 pm »
The Bud case is very nice and very well made, also expensive.  I used a TR6102 for my winding machine controller and the last time I checked they had jumped to $225.00 (about $100 higher than they used to be).  Yipes, I just checked latest pricing and they're up to $275.00, ridiculous.  I did find a 'discounted' price of $244 at one place, still pricey.

They can be found here for $174;
http://www.aiconsol.com/tr-6100-bud.html

Still not cheap, but I wanted to make this a nice piece of equipment I could admire for years, and I'm having a blast building and learning.
« Last Edit: July 11, 2017, 11:42:02 pm by kj7e »
 

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Re: KX Reference
« Reply #84 on: July 11, 2017, 11:04:53 pm »
kj7e: nice build. Thanks for the info on the case. What are you planning for the output protection (short circuit, feeding in voltage, maybe gas discharge tube)?

The output buffer is going to be the LTC1150/LT1010 combo. The LT1010 is fairly robust and can withstand shorts and other abuse;
http://cds.linear.com/docs/en/datasheet/1010fe.pdf
 

Offline SvanGool

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Re: KX Reference
« Reply #85 on: July 11, 2017, 11:10:01 pm »
@KJ7E:

Nice design !

If you want this to be an "easy" travelling standard, without the need of guiding "dangerous goods" documents/labels (and the risk that your post/freight company won't take it as a standard package), one cell needs to be below 20 Wh (that was the easy part) and your total battery (consisting of one or more cells) capacity needs to be below 100 Wh (that is the difficult part) and you cannot have more than 4 cells or two batteries, according IATA Battery guidance 2017 for air freight UN3481 PI (Package Instruction) 967 Section II . If you are able to accommodate that, then that would make your solution fly.  :)

In another project, I was looking for 8x (4S2P) Samsung INR18650-35E (12.24 Wh according official Samsung specs), which just fits the bill.

I am curious, can you give some more detail on your oven control circuitry?
# Don't hurry, the past will wait. #
 

Offline kj7e

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Re: KX Reference
« Reply #86 on: July 11, 2017, 11:25:30 pm »
@KJ7E:

Nice design !

If you want this to be an "easy" travelling standard, without the need of guiding "dangerous goods" documents/labels (and the risk that your post/freight company won't take it as a standard package), one cell needs to be below 20 Wh (that was the easy part) and your total battery (consisting of one or more cells) capacity needs to be below 100 Wh (that is the difficult part) and you cannot have more than 4 cells or two batteries, according IATA Battery guidance 2017 for air freight UN3481 PI (Package Instruction) 967 Section II . If you are able to accommodate that, then that would make your solution fly.  :)

In another project, I was looking for 8x (4S2P) Samsung INR18650-35E (12.24 Wh according official Samsung specs), which just fits the bill.

I am curious, can you give some more detail on your oven control circuitry?

Not too worried about shipping here in the US, just have to send it UPS or FEDEX ground.  I wanted the capacity and the LiPo's where inexpensive (Hobby King).

Back a page, I posted some more info on the oven control circuit, here is the post;
https://www.eevblog.com/forum/metrology/kx-reference/msg1241349/#msg1241349
I have to admit, it works better than I could have hoped for.
 
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Offline Edwin G. Pettis

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Re: KX Reference
« Reply #87 on: July 12, 2017, 01:33:41 am »
KJ7E,

I checked out the link, the $174 is for the 6100 and they don't seem to have the TR-6102 listed.  Back in the day when I bought this unit for the controller, it was a 'paltry' $125.00 and that was expensive back in the latter '90s.  The TR-6102 actually cost more than the PCB and all the components on it, the PCB is about 12.5" L x 7" W.  Now, that case is close to >2.5 times the components.
 

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Re: KX Reference
« Reply #88 on: July 12, 2017, 06:09:19 pm »
KJ7E,
Head's up using LT1150 / '1010 on a Vref.  Watch your noise density specs on the '1010 especially and the '1150 is a pretty slow & noisy chopper compared to newer designs - those parts are ancient history these days and will splatter noise downstream if you're careful.  I would use a simpler, cheaper 10-cent transistor follower output drive circuit over a '1010 for much lower noise - IF you don't need push-pull output current.  It just depends on what you'll use this for.

I suggest you test the output circuit very carefully to make sure it's what you need and matches up to what you can measure (or not).
 
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Offline kj7e

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Re: KX Reference
« Reply #89 on: July 12, 2017, 07:02:40 pm »
KJ7E,
Head's up using LT1150 / '1010 on a Vref.  Watch your noise density specs on the '1010 especially and the '1150 is a pretty slow & noisy chopper compared to newer designs - those parts are ancient history these days and will splatter noise downstream if you're careful.  I would use a simpler, cheaper 10-cent transistor follower output drive circuit over a '1010 for much lower noise - IF you don't need push-pull output current.  It just depends on what you'll use this for.

I suggest you test the output circuit very carefully to make sure it's what you need and matches up to what you can measure (or not).

I'm open to suggestions,  without derailing this thread too much, what would you recommend over the 1150?  I was just basing this on LT App note 86 page 46.
 

Online The Soulman

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Re: KX Reference
« Reply #90 on: July 12, 2017, 07:51:33 pm »
It appears to me that we have some very knowledgeable people here, is it possible for them to write up a recipe with
today's best parts and practices?
With so commentary on how and if and such.
And perhaps make that a sticky so they won't have to answer these questions every couple of weeks.  ;)
 

Offline lukier

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Re: KX Reference
« Reply #91 on: July 12, 2017, 08:49:19 pm »
I guess the answers are probably in the LTZ1000 thread :D
 

Offline hwj-d

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Re: KX Reference
« Reply #92 on: July 12, 2017, 09:03:41 pm »
KJ7E,
Head's up using LT1150 / '1010 on a Vref.  Watch your noise density specs on the '1010 especially and the '1150 is a pretty slow & noisy chopper compared to newer designs - those parts are ancient history these days and will splatter noise downstream if you're careful.  I would use a simpler, cheaper 10-cent transistor follower output drive circuit over a '1010 for much lower noise - IF you don't need push-pull output current.  It just depends on what you'll use this for.

I suggest you test the output circuit very carefully to make sure it's what you need and matches up to what you can measure (or not).

I'm open to suggestions,  without derailing this thread too much, what would you recommend over the 1150?  I was just basing this on LT App note 86 page 46.

Because i'm learning this stuff at the moment, that's a very interesting question to me too. I also orient myself to this old but very informative documents (Jan 2001). Are there comparable practice-oriented Infos like this for newer designs with modern Op Amps out in the net?

OT: Agree with The Soulman, it would really help- and thankful, if someone could explain in short these differences to modern chips on the market. Specially in relation to use them with references.
 

Offline Muxr

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Re: KX Reference
« Reply #93 on: July 12, 2017, 09:26:11 pm »
I guess the answers are probably in the LTZ1000 thread :D
From my reading at least as far as LTZ1000 is concerned, there are two schools of thought, when it comes to which Op Amps to pair LTZ1000 with.

- modern chopper LTC2057 (this is what TiN's KX uses)

- or the conventional LT1006, LT1013 (dual) which LTZ1000 specifies in the datasheet and Linear recommends.
 

Offline lukier

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Re: KX Reference
« Reply #94 on: July 12, 2017, 09:57:58 pm »
From my reading at least as far as LTZ1000 is concerned, there are two schools of thought, when it comes to which Op Amps to pair LTZ1000 with.

- modern chopper LTC2057 (this is what TiN's KX uses)
- or the conventional LT1006, LT1013 (dual) which LTZ1000 specifies in the datasheet and Linear recommends.

Well that's just the opamp for the LTZ1000 circuit itself and I must say MisterDiodes' arguments (from some other thread) against LTC2057 seem sensible.

Here, especially in case of a nice box-standard build, like KJ7E does (not just the PCB with LTZ1000 page 6 circuit) I would be interested in the output buffer and the related protections. Frying LTZ1000 is something I would really like to avoid :)

Fluke 732B schematics offer some hints. They seem to have some diode and TVS across the output along with some capacitors, gas discharge tube from LO to earth and something that looks like transistor short circuit protection (Q1,C1,Q2,R1) and voltage clamp (CR1), see A2 flex circuit PCA and A1 front panel PCA schematics.
 
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Offline hwj-d

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Re: KX Reference
« Reply #95 on: July 12, 2017, 10:28:31 pm »
Quote
I would be interested in the output buffer and the related protections.
That's the point.
 

Offline TiN

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Re: KX Reference
« Reply #96 on: July 13, 2017, 12:27:01 am »
Meanwhile I'm getting VK5RC's KX reference ready for shipment back to Oz cal-club.

Before





Tempco is bad, expected below 0.05ppm/K, typical to LTZ ref.

After

I didn't quite like the way board was mounted, so I got it free hanging, surrounded by foam. Then rewired copper junction from zener opamp to match B03 PCB version (VK5RC used older B01 in his build). And dropped LTZ package flush to the board, instead of standing on the legs. As result output shifted -15ppm.

Note different PPM scale +1/-1ppm instead of 0/-3ppm on first graph.



Yay, tempco is beyond measurement ability of K2002 over 17C deg span. As expected.

And since no thread is good without photos, here they are:



CSV data as usual Run 1, Run 2, started Run 3 with slower ramp.

Now just need to get final calibration using 4 of my meters, and it's finally ready to go to VK5RC next monday.  :-+
« Last Edit: July 13, 2017, 12:37:16 am by TiN »
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Offline VK5RC

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Re: KX Reference
« Reply #97 on: July 13, 2017, 11:17:00 am »
Thanks for your efforts TiN,
Interesting results, I take from it,
1 Mr Pettis makes nice resistors, esp in value compared to Vishay,
2 The 2057 does quite well,
3 Is the LTZ 1000 especially vulnerable to air currents from below? 
4 The changes of Kx board  from B01 to B03 important.
5 You can mount wire wound type resistors in the vertical fashion without too much compromise.
6 The mounting of the Kx board is best by foam suspension. - I need to take the covers off the 3458 and see how HP mounted their LTZ. I recall? 2 lots of pin headers, but poss other mechanical fixtures .

Again thanks, once back, I will look at how far off my 3458 is, and then forward it around the Aus Cal Group.
Regards Rob 
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Offline julian1

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Re: KX Reference
« Reply #98 on: July 15, 2017, 02:34:53 am »
I like it. What is the case model? It seems perfect size for such kind of project. Next step to put some Raspberry Pi inside for datastorage/logging and external meter control, so you can always keep digital history of the reference together with the box, making it perfect travel standard.

Bud Industries TR-6100;
http://www.budind.com/view/Small+Metal+Electronics+Enclosures/TR+Series+Small+Cabinet

If you search around you they can be found at a discount.  The Die Cast box used for the oven/shielding is a Bud Industries CU-4234.  The Raspberry Pi with environmental logging is a good idea, maybe for V2.  Once this one is built, I hope to send it off to someone with a freshly calibrated 3458A or better to measure/adjust.

Is the carrying handle/tilting bail aluminium or plastic? It looks like it might be a bit fragile if plastic.
 

Offline kj7e

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Re: KX Reference
« Reply #99 on: July 15, 2017, 03:10:59 am »

Is the carrying handle/tilting bail aluminium or plastic? It looks like it might be a bit fragile if plastic.

Aluminum, with a neoprene wrap.  Includes Teflon washers and nice three prong adjustment knobs as well.
 
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Offline mimmus78

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Re: KX Reference
« Reply #100 on: July 15, 2017, 09:06:14 am »
So my KX REFERENCE has turned 6m old. It's still stable in respect to my 3458a. I expected some seasonal drift but both 3458a and KX are still rock solid to the 0.3ppm.

Reference was almost constantly power on during this 6m and 3458a was used around 20% of time. As I already explained I noticed a 1ppm drift few months ago in both 3 reference, so this was connected to my 3458a that is still running hot.

I noticed this KX seems to drift up, while the other two LTZ reference exhibit the 1ppm down shift during first month as stated in datasheet.

Also my other two LTZ1000 references seems stable (but they are not constantly powered on) but in last months I didn't have much time to dedicate to this ...

Anyway what are changes from B01 to B03?
 

Offline hwj-d

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Re: KX Reference
« Reply #101 on: July 15, 2017, 09:44:14 am »
So my KX REFERENCE has turned 6m old. It's still stable in respect to my 3458a.
...

Are there somewhere photos in the forum i.e. which resistors you use? Thanks.
 

Offline Andreas

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Re: KX Reference
« Reply #102 on: July 15, 2017, 04:18:23 pm »

I noticed this KX seems to drift up, while the other two LTZ reference exhibit the 1ppm down shift during first month as stated in datasheet.


Does it really drift up or only slower down than the other references.
Usually a LTZ drifts down.
The real drift can only be determined by comparison with official calibrated instruments over several years.

With best regards

Andreas
 
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Offline mimmus78

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Re: KX Reference
« Reply #103 on: July 15, 2017, 05:03:29 pm »
So my KX REFERENCE has turned 6m old. It's still stable in respect to my 3458a.
...

Are there somewhere photos in the forum i.e. which resistors you use? Thanks.

No I think I didn't have photos ... and I have no plans to open it right now.

Anyway I used many tht parts, so it's not to be taken as reference, nothing to be proud of and a little bit delicate too. I also think because of this is also almost unshippable without risking upsetting it.

I used LT1006 as op amp (single version of lt1013), Edwin resistors, it's buffered by a simple 2057, some caps and ferrite beads to avoid EMI.

I used an external wall wart transformer (to avoid disturbances) and a 15V linear regulator inside the metallic case.

A small resistor was also added to add some more capacitative load driving capabilities after the buffer.

If you search among Andreas posts you'll find anything I did.


So my KX REFERENCE has turned 6m old. It's still stable in respect to my 3458a.
...

Are there somewhere photos in the forum i.e. which resistors you use? Thanks.


Inviato dal mio Nexus 6P utilizzando Tapatalk

 
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Offline mimmus78

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Re: KX Reference
« Reply #104 on: July 15, 2017, 05:06:24 pm »

I noticed this KX seems to drift up, while the other two LTZ reference exhibit the 1ppm down shift during first month as stated in datasheet.


Does it really drift up or only slower down than the other references.
Usually a LTZ drifts down.
The real drift can only be determined by comparison with official calibrated instruments over several years.

With best regards

Andreas
Andreas this is reason I added the word "it seems".

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Offline TiN

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Re: KX Reference
« Reply #105 on: July 16, 2017, 10:53:28 pm »
I think it's all done for VK5RC's reference and it's ready to go now.

Here I cooked little calibration report with the data I got.
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Offline kj7e

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Re: KX Reference
« Reply #106 on: July 16, 2017, 11:24:10 pm »
I think it's all done for VK5RC's reference and it's ready to go now.

Here I cooked little calibration report with the data I got.

Nice report!
 

Offline Andreas

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Re: KX Reference
« Reply #107 on: July 17, 2017, 04:44:24 am »
Hello Illya,

in the report you state 7K BMF in series with the reference for noise measurement.
Together with the 1K input resistance this will give a 8:1 voltage divider for the noise voltage.

Is this regarded on the measurement?
I usually short the series resistor after charging up the input capacitors of the noise amplifier.

With best regards

Andreas
 

Offline VK5RC

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Re: KX Reference
« Reply #108 on: July 17, 2017, 07:32:47 am »
Hi TiN,
Thank you for your efforts with this reference and publishing this and your other experiments results.
My 3458a is warming up, down here in south Australia the ambient air temp is not 24C at present, but I can reproduce this and other environmental conditions.

Over the weekend I had everything warmed up (22C), including the room everything is in, the 3458 and my 731 (both are pretty old) , I am getting results consistent with readings from 6 months ago to within 3uV.

The reference will be allowed to settle here for a while - while I check my dmms (3458, 3457, 34461) then off for a 'road trip'  around the Aus Cal group, one has an 'in cal' Keithley  7510.

I think the best place to show the data will be on the Calibration Group post. I will post mine there and link to your results as well.

I was glad to see about 100 of your 'Kx babies' are out in the world! You should be a proud 'father'.
My next project (about 2/3 complete)  is 6 Kx boards for a long term references study.

Again thanks,
Robert
VK5RC
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Offline Jon.C

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Re: KX Reference
« Reply #109 on: July 18, 2017, 12:28:35 pm »
hi

It is possible to buy all the components in a kit to mount ?
 

Offline VK5RC

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Re: KX Reference
« Reply #110 on: July 18, 2017, 12:58:28 pm »
Hi Jon,
I know of no kit. You can assemble the bits yourself though.
xDevs (TiN) has on his website a list of the common parts from DigiKey - he even has the Digikey part numbers. Thanks TiN.
A PCB is available through OshPark PCB - see link on xDevs website.
The good resistors (the 120R, 1K, 70k x2 and the 12 to 13k) are the tricky part - Vishay's very good resistors are very expensive and hard to source easily esp in Australia, Mr Pettis (Ultrohm) USA has some very nice wire wounds for a very good price - he is busy. Some other wire wound  resistors made by TE, model UPW50 can be sourced (In Australia) through RS components but to get the values a bit of mixing is required.
The LTZ1000 can be got through DigiKey, they have the C model in stock at present , I recently sourced some A models through TME. Others have got a few from the manufacturer directly - I have not done this. Cabling, mounting/boxing/insulation, power supply etc are other decisions

Half the 'fun' is researching what you want to get out of this, how much you want to spend, what you can get. I don't know what is available/import issues in your country - this can make a big difference on choices.
Every decision you make has some impact between $, long term stability, noise, ambient air temp etc. Look at the variation in the completed Kx references presented on this website to date - almost no 2 are identical.
Some of the serious Volt-Nut guys  on this website have given a lot of time , experience and knowledge away - worth quite a bit of reading!
Regards Robert (volt-nut trainee!)
Whoah! Watch where that landed we might need it later.
 
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Offline SvanGool

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Re: KX Reference
« Reply #111 on: July 18, 2017, 02:04:45 pm »
Not as good as Mr Pettis resistors and the Vishays, I found a supplier of NOS (New Old Stock) Sfernice RCK02 0.5W 5ppm/C (good enough for the LTZ1000) precision foil resistors who supplies directly from stock:
I have them here and they are fine, although you do have to bend, one of the leads, a little bit to fit the KX PCB.

Ready for action:


« Last Edit: July 18, 2017, 09:07:52 pm by SvanGool »
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Offline RandallMcRee

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Re: KX Reference
« Reply #112 on: July 18, 2017, 06:54:59 pm »
If we are going for best price-to-ppm on the cheap side then consider the PTF56 (Z) series--they are spec'ed at 5ppm and are reasonably priced. Mouser has enough in stock that you can get correct values by putting two in parallel or series where needed.

E.g 1Kohm:
http://www.mouser.com/ProductDetail/Vishay-Dale/PTF561K0000BZEK/?qs=sGAEpiMZZMu61qfTUdNhG3EzrPz99APhc7QJ%252bu1T2BQ%3d

I'm new at this, so please tell me if these are known to not meet their specs, for example.
 
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Online Kleinstein

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Re: KX Reference
« Reply #113 on: July 18, 2017, 07:15:22 pm »
PTF56 is lower price, but the drift and similar rating a about an order of magnitude worse than the foil resistors. I know comparing typical number is somewhat tricky and not that reliable - but at least in this case both number are from a common source.
For a reference used in a lab, the TC is usually not that important it is more about the less controlled parameters like humidity.
Drift of the PTF56 (e.g. 400 ppm load life, 800 ppm moisture) might be still visible after attenuation (factor 100-500) through the LTZ1000 circuit.
 
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Offline kj7e

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Re: KX Reference
« Reply #114 on: July 23, 2017, 08:37:26 pm »
The portable oven enclosure is done.  Built a compact 20v 500mA linear supply so I would not have to tie up or keep a lab supply on all the time.  The output is surprisingly clean.















Got lucky with the MC78M20CT regulator, 20.000v


And clean, >3Hz filter;





 
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Online Vgkid

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Re: KX Reference
« Reply #115 on: July 23, 2017, 09:17:40 pm »
Nice job.
Do you have a schematic for the heater?
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Offline kj7e

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Re: KX Reference
« Reply #116 on: July 24, 2017, 12:07:18 am »
Nice job.
Do you have a schematic for the heater?

Back two pages, but I need to upload an updated version, slight changes, replaced the 499k negative feedback resistor for 2M Ohm for more gain (started to oscillate at 4M Ohm), also using a second 10K NTC disk type sensor in series with the oven chassis mounted sensor to better average the real internal air temp and the series resistor value was changed with the temp set pot due the second series temp sensor.  The oven internal air temp stays within about 0.3 deg C from 15 deg C to 30 deg C ambient.  About the best I could do with out going crazy.  Have some thoughts on experimenting with an Arduino with both hysteresis and predictive compensation, maybe on v2.
« Last Edit: July 24, 2017, 03:32:02 am by kj7e »
 

Online Kleinstein

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Re: KX Reference
« Reply #117 on: July 24, 2017, 08:27:10 pm »
For good temperature regulation it would help if there is a temperature sensor relatively close to the heater. Fast reaction of the sensor help making the loop stable and thus allows a higher gain. It could also help to use an PI or maybe even PID regulator. One way to combine a sensor close to the heater and a second closer to the circuit is to use the first sensor for the P and D part and the second sensor for the I part only. However an analog PID could be tricky, due to the long time constants.

Another point is that the resistive heater makes it nonlinear. So the temperature regulator loop gain is higher, the higher the heater power. It would be possible to avoid this, by using the transistor as the heater instead of the resistors. As a side-effect this is also more energy efficient.
 
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Offline kj7e

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Re: KX Reference
« Reply #118 on: July 24, 2017, 09:45:25 pm »
For good temperature regulation it would help if there is a temperature sensor relatively close to the heater. Fast reaction of the sensor help making the loop stable and thus allows a higher gain. It could also help to use an PI or maybe even PID regulator. One way to combine a sensor close to the heater and a second closer to the circuit is to use the first sensor for the P and D part and the second sensor for the I part only. However an analog PID could be tricky, due to the long time constants.

Another point is that the resistive heater makes it nonlinear. So the temperature regulator loop gain is higher, the higher the heater power. It would be possible to avoid this, by using the transistor as the heater instead of the resistors. As a side-effect this is also more energy efficient.

Yep, I found that out.  Also mounted the heater element pass transistor to outside front of the oven for added efficiently and this also helps heat a third side.  I had some extra 10K NTC sensors laying around so I started experimenting again today and may have made vast improvement.  Currently, the heater resistors are on the ends | ----- | of the oven, one sensor was mounted just offset from the left resistor.  This gave great and stable feedback and the area near the resistor stayed at a very consistent temp.  Where I found some variation is with the internal air temp due to the top, bottom, front and back of the oven not being heated and only relying on the conductive heat from the left and right sides.  Better insulation would help, but there is no more room for more insulation in the box.   So my idea was to place the oven body temp sensor center bottom of the oven,  this surface, while insulated, is in contact with the bottom cover of the box.  I figured this area would be more representative of the internal air temp and the most effected by ambient change.  So far I'm able to hold the internal air temp well within 0.1 dec C from the same 15-30 dec ambient.  The downside is a bit more initial oscillation and time to stabilize, but it seems to be a good trade off.  Ill post of some temp plots and sensor locations after more testing.
 

Online Kleinstein

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Re: KX Reference
« Reply #119 on: July 25, 2017, 07:20:39 am »
I would consider a temperature stable to 0.1 C already quite good for a reference circuit that is by its own not very sensitive to temperature.

If one uses the transistor as a heater, it might be a good idea to replace the heater resistors also with constant voltage heater, like zener diodes or maybe a transistor in a VBE multiplier circuit. This way the distribution of the heat sources would be approximately fixed.

With better insulation, there is also a downside: the minimum temperature for the circuit will increase.

For monitoring the temperature of the reference circuit, one could watch the heater current needed by the LTZ1000 circuit. Ideally this would be constant at a not to low level - at low power levels the regulation of the LTZ1000 circuit is expected to get less accurate as the loop gain in going down.
 
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Online The Soulman

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Re: KX Reference
« Reply #120 on: July 25, 2017, 09:03:37 am »
@kj7e, how do you transport the 10V dc from inside to outside the oven?
Long wires with the additional length coiled up inside and outside the oven to minimize temperature gradients across
the (inevitable) solder connections?
 

Offline kj7e

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Re: KX Reference
« Reply #121 on: July 25, 2017, 02:38:49 pm »
@kj7e, how do you transport the 10V dc from inside to outside the oven?
Long wires with the additional length coiled up inside and outside the oven to minimize temperature gradients across
the (inevitable) solder connections?

That is a good question and one I have been wondering myself.  After some further review I still feel the LTC1150/LT1010 buffer will suit me the best.  The buffer board will be in the oven as well.  From the buffer will be a pair of 24 awg solid copper ptfe twisted pair wires to the Pomona 3770 binding posts.  One pair for the LT1010 10v output and one pair for the LTC1150 feedback or ratio set.  Here is a diagram I found showing the buffer kelvin wires and ratio set (thank you Simon);
http://satcom.tonnarelli.com/files/LTZ1000A/NxtGenOpAmpBoard(RevA).pdf

The wires will pass though the oven via small holes with rubber grommets, there will be a few inches of wire in a semi coil to the front panel binding posts (see the third photo down in my post above) to facilitate assembly/disassembly and maintenance.  I know there will be a slight temp gradient from the oven to the binding posts.  What I don't yet understand well is how to best minimize the thermal emf between the output and binding posts.  Such as, if the thermal gradient is minimized in solid copper wire from one solder point to the next, will that effectively minimize the thermal emf?   I have some reading to do. 
« Last Edit: July 25, 2017, 02:45:43 pm by kj7e »
 

Online Kleinstein

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Re: KX Reference
« Reply #122 on: July 25, 2017, 03:10:38 pm »
For the thermal emf it depends on the material where the the temperature gradient is in. So ideally there will be a relatively long copper wire (e.g. twisted pair) from the oven to the outside, with quite some length of wire with good thermal contact both in the oven and at the outside near the terminals. So the setup seems to already quite good. Usually there should be no need for Teflon isolation, as the lines are low impedance. If paranoid or in a really sensitive circuit like a nV amplifier one should avoid bending the wires in the temperature gradient part. In case of separate drive and sense lines, it is the thermal emf in the sense lines that matters.

Normally I would avoid having the buffer inside the oven - it adds extra power and a good buffer should be stable even without a stable temperature. However the place inside might be more convenient for EMI reasons. If there is 7 to 10 V scaling, it is of cause important to have at least the resistors at constant temperature. However in this case is might be convenient to have both a 7 V and a 10 V output.

The amplifier circuit linked is sensitive to extra resistance in the sense wires. So one might have to find a good compromise in wire length between the extra resistance and thermal emf errors. One might consider unequal lengths of wire, so to get the same about 2:1 ration for the resistance. One also has to take care about the supply current (especially for the reference) - it might need an extra current compensation.
 
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Offline hwj-d

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Re: KX Reference
« Reply #123 on: July 27, 2017, 02:35:58 pm »
At this point a lightly philosophical question:

Why or for what we need this special exact 10V output there?
 
Isn't it better to let the generated 7.xxxxxxxxxxxV be there as buffered output as it is, but instead build a additionally ADC DAC buffered precise output for variable voltages as we need in real live, like IanJ with his PDVS2 does?
« Last Edit: July 27, 2017, 04:33:15 pm by hwj-d »
 

Offline Echo88

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Re: KX Reference
« Reply #124 on: July 27, 2017, 08:29:51 pm »
Youre right that the 7.xV output is more stable, but with 10V you can (theoretically!) calibrate a 3458A and its a nice round value to work with. You mean a PWM-based DAC like the Fluke 5700 PWM-DAC? Thats a glorious design for sure. But nobody has yet designed a open source pcb based on it. Apart from the fact that it doesnt produce a 10V as stable over time as a Datron 4910-Design for example.
 

Offline TiN

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Re: KX Reference
« Reply #125 on: July 28, 2017, 12:38:04 am »
You can calibrate 3458 off 7.xx volt too.
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Offline MisterDiodes

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Re: KX Reference
« Reply #126 on: July 28, 2017, 04:44:24 pm »
Correct - in the real world you want an LTZ to provide a very stable non-zero voltage reference, anything you do to that Vref to boost or attenuate that reference is going to add noise, drift and overall instability.   We find that we need a meaningless 10V cardinal point less and less - although it is very important to know WHAT absolute value you have on your Vref.

Again:  The LTZ circuit is really very easy compared to an ultra-stable 10V boost circuit (732a/b level) - normally if you're dealing with ADC's or DAC you want to divide the 7.XXXXX zener voltage, not boost it.  Boost circuits will always tend to add more drift and noise no matter what, because generally you're gaining up any circuit errors.  Just depends on what your application needs.

If you really -need- a 10V calibration reference, it's much easier, reliable and profitable to just use (or rent or borrow) a calibrated 732a/b - and keep it calibrated - if your time is worth anything and you're on the clock. I know it's not as fun, but that's reality.  Especially if you have to pass an ISO900x audit: a self built reference (non-JJA) will probably never pass muster anyway (not for less $$$ than a 732), no matter how good it is.
« Last Edit: July 28, 2017, 09:19:43 pm by MisterDiodes »
 
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Offline lukier

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Re: KX Reference
« Reply #127 on: July 28, 2017, 05:03:57 pm »
You can calibrate 3458 off 7.xx volt too.

Does anyone know if Fluke 5440B (I'm now repairing one, will take a while, some DIY needed) can also accept 7.x for the external 10V cal? In the operator and service manuals it only says:
Quote
If the voltage standard is not exactly 10V, the exact value may be entered at this time with the numeric DATA ENTRY keys.

But I have no idea if the software imposes limits (e.g. only from 9 to 11V).
 

Offline kj7e

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Re: KX Reference
« Reply #128 on: August 05, 2017, 03:58:07 pm »
Full scale on the 34465a is 27 Ohm, with the 10K thermistor (U.S. Sensor USP10976) this comes to ~0.1 deg C full scale.   Internal oven air temp vs external ambient air temp, starts at 24 deg C ambient at 9am.  As the ambient temp started to drop so did the internal air temp, but only by about +5 Ohm or -0.02 deg C at the 35 min mark.  As the ambient temp fell further down to 15 deg C at 12pm the internal air temp raised by -10.5 Ohm or + 0.04 deg C. The climb back to room temp shows a slight negative overshoot with the internal before the steep rise in internal temp as the external ambient temp climbed over 30 deg C, however still staying within +.05 deg C.  So 15 deg C to 30 deg C ambient the internal air temp is within + or - 0.1 deg C, close enough.  Note, the two plots are askew time wise.




About 15 weeks after my order, look what showed up yesterday;



I revised my mounting method and carved out some open cell foam;





With the proper resistors, the voltage is now 7.14150, up from 7.13358 where it has been burning in for the last two months.   I noticed no real change or drift from 25 deg C with the oven off to 35 deg C with the oven on.  Now I have the proper voltage, I can order the resistor network for the buffer.

I don't need 10v for any specific reason, I don't even need this reference to to tell you the truth.  This is just a project I wanted to build, for the fun of it.
« Last Edit: August 05, 2017, 05:07:11 pm by kj7e »
 
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Offline Muxr

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Re: KX Reference
« Reply #129 on: August 05, 2017, 08:55:28 pm »
It's been almost a month since I ordered a LTZ1000A for my 2nd LTZ1000A reference, and it still hasn't shipped. Looks like they are really out of stock.  :(
 

Offline kj7e

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Re: KX Reference
« Reply #130 on: August 05, 2017, 09:20:30 pm »
It's been almost a month since I ordered a LTZ1000A for my 2nd LTZ1000A reference, and it still hasn't shipped. Looks like they are really out of stock.  :(

Through Digikey?  They say ship date for the "A" is Sep 16th, they have the non "A" in stock.
 

Offline Muxr

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Re: KX Reference
« Reply #131 on: August 05, 2017, 10:04:50 pm »
It's been almost a month since I ordered a LTZ1000A for my 2nd LTZ1000A reference, and it still hasn't shipped. Looks like they are really out of stock.  :(

Through Digikey?  They say ship date for the "A" is Sep 16th, they have the non "A" in stock.
From LT directly. Yeah I know non A is in stock, I wanted to build an A version, since I already have an non-A one.
 

Offline cellularmitosis

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Re: KX Reference
« Reply #132 on: August 06, 2017, 04:20:13 am »
It's been almost a month since I ordered a LTZ1000A for my 2nd LTZ1000A reference, and it still hasn't shipped. Looks like they are really out of stock.  :(

I decided to take a risk on some used units from hifi-szjxic.  He has them in stock :)

http://www.ebay.com/itm/1x-LTZ1000ACH-Ultra-Precision-Reference-LTZ1000A-/111325506311

I haven't yet verified they are legit / working.

LTZs: KX FX MX CX PX Frank A9 QX
 
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Offline VK5RC

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Re: KX Reference
« Reply #133 on: August 06, 2017, 04:24:14 am »
Re LTZ 1000A, I got one from TME, a bit more than Digikey but posted really quickly.
Whoah! Watch where that landed we might need it later.
 
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Offline TiN

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Re: KX Reference
« Reply #134 on: August 06, 2017, 05:16:56 am »
Look legit to me.
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Offline kj7e

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Re: KX Reference
« Reply #135 on: August 06, 2017, 05:31:53 am »
I have a nice TE, PTFE socket for the LTZ1000 if you want it.  Also one extra KX board.
 

Offline BU508A

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Re: KX Reference
« Reply #136 on: August 07, 2017, 11:38:01 am »
“Chaos is found in greatest abundance wherever order is being sought. It always defeats order, because it is better organized.”            - Terry Pratchett -
 

Offline kj7e

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Re: KX Reference
« Reply #137 on: August 07, 2017, 06:40:12 pm »
One hour plot of the KX LTZ1000A with the Keysight 34465A (best I have).  I was fighting Excel trying to get both plots on the same chart, I was spending too much time on and gave up.  All this shows is the tempco sensitivity of the 34465A.  Hard to keep the room any more consistent in temp, the LTZ1000A was held steady at 35 deg C while the 34465A was subject to the ambient temp.

« Last Edit: August 08, 2017, 06:36:44 pm by kj7e »
 
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Offline kj7e

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Re: KX Reference
« Reply #138 on: August 08, 2017, 12:25:51 am »
@TiN,

I'm seeing 7 to 8uV downward drift as the KX reference warms up from 20 deg C to 35 deg C,  is that about whats expected or does that seem excessive?  Reading back to your post about VK5RC's board, one of the tempco improvements you made was with dropping the chip to the board.  I'm wondering if I should do the same now.  If I take 0.05ppm/C I should see less than 6uV for 15 deg C change.

« Last Edit: August 08, 2017, 01:42:14 am by kj7e »
 

Online Kleinstein

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Re: KX Reference
« Reply #139 on: August 08, 2017, 11:34:27 am »
The 7-8 µV are about the normal order of magnitude, though it can depend on the resistors used. In the unit with extra temperature stabilization this is not at all problem, as the more normal temperature change will be much smaller.

The change in TC when changing from some distance to the board to short pins is somewhat predictable. So before shortening the pins one should look at the sign of the TC, as the small change could also be to the wrong direction. I think Andreas did a few tests on the TC with short and long pins.

 
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Offline kj7e

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Re: KX Reference
« Reply #140 on: August 08, 2017, 03:29:51 pm »
The 7-8 µV are about the normal order of magnitude, though it can depend on the resistors used. In the unit with extra temperature stabilization this is not at all problem, as the more normal temperature change will be much smaller.

The change in TC when changing from some distance to the board to short pins is somewhat predictable. So before shortening the pins one should look at the sign of the TC, as the small change could also be to the wrong direction. I think Andreas did a few tests on the TC with short and long pins.

I remember reading about that when I was searching for lead length info some months back.  It was discussed around here; https://www.eevblog.com/forum/metrology/ultra-precision-reference-ltz1000/msg928435/#msg928435

It seems, the shorter leads reduce the downward drift with rising temp.  My chip is maybe 1.5mm above the board now, so I could shorten the leads some.  First I'm going to see if the drift is repeatable a few times then I think I'll try trimming the leads.
 

Online Kleinstein

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Re: KX Reference
« Reply #141 on: August 08, 2017, 05:23:48 pm »
With very short leads, there is also more transfer of board stress towards the reference. The linked thread also has the comment that a 1 mm spacing is suggested. So not very much change from the now 1.5 mm. So I would not bother and not add new stress from soldering.  The extra box with heats should reduce external temperature variation quite a lot - cold be about  a factor of 100 if I understand the curves right. So the TC of the reference is less critical than in a normal circuit without the extra heater.

The downside of the external heat is that the internal heater is working at a relatively low power level. Due to the square law heater this means slightly less accurate temperature regulation. So one might be tempted to slightly adjust the temperature regulation circuit for better operation at low power: Increase the loop gain and add some kind of nonlinear approximation of the square root function to reduce the gain again at high power.
 
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Offline MisterDiodes

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Re: KX Reference
« Reply #142 on: August 08, 2017, 07:11:44 pm »
A few quick thoughts:

A)  With that meter and temperature range, you have to allow for the meter drift that takes place over the same time and temp range.  I don't think you're measuring accurate uV like you think you are - but otherwise nothing to be alarmed about.  Look out also for thermals and offsets developing across every connection while ambient conditions change.  You'll want an equipment upgrade in the future to chase into low PPM territory like you want to - this is where nulling against a stable Vref/s like 732a/b + KVD + null meter can help you get down into the finer details of accurate lower ppm measures better and faster than a DMM.  Heck, you can grab a couple null measures against a couple 732's just while a 3458a is still running AutoCal  :)  We use all techniques though to get the best quality measure.

Lead length should make no huge difference on "A" version in terms of board stress - the leads are fairly isolated from board stress with the wire bond layout inside that package - that's another change request by HP for the "A" version decades ago.  The non A version might be a bit more tender; we never use those.  We just put those "A" right down onto the PCB, and we don't run them especially cold either - they are fine after decades (13k over 1k minimum heater resistor ratio).  What you can have happen is -any- exposed lead length can make a spot  where air currents cause all sorts of problems.  You want that package protected from air currents, especially the leads (top and bottom).  That is not the same thing as over-insulating it, which is worse.

B)  I wouldn't ever use sockets unless you want to just do a quickie initial parts test.

C)  Watch out for eBay suppliers of LTZ.  For the cost of the rest of the system I'd just go with ordering from LT direct - yes it takes several weeks sometimes but that's lowest risk. Right now there are zero eBay suppliers selling -confirmed- factory prime parts...everything you see listed is some sort of floor sweeping reject.  They might work or they might be out of spec.  For the cost of the parts I want to give it best chance at lowest risk.  Right now LT direct is quoting del'y about September or so.

 
« Last Edit: August 08, 2017, 07:13:45 pm by MisterDiodes »
 
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Offline Andreas

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Re: KX Reference
« Reply #143 on: August 08, 2017, 07:12:31 pm »
I'm seeing 7 to 8uV downward drift as the KX reference warms up from 20 deg C to 35 deg C,
Hmm,

is this the drift of the zener or from the DMM (warm up drift) or some ageing drift?
I usually do a complete temperature cycle to see if there is something fishy in the measurement setup.
And from the 5 connected measurement devices sometimes there is one which does not agree to the others.

with best regards

Andreas

 
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Offline kj7e

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Re: KX Reference
« Reply #144 on: August 08, 2017, 07:29:17 pm »
I'm seeing 7 to 8uV downward drift as the KX reference warms up from 20 deg C to 35 deg C,
Hmm,

is this the drift of the zener or from the DMM (warm up drift) or some ageing drift?
I usually do a complete temperature cycle to see if there is something fishy in the measurement setup.
And from the 5 connected measurement devices sometimes there is one which does not agree to the others.

with best regards

Andreas

The DMM has been powered on for 21 days and is staying within 0.5 deg C while the KX-LTZ1000A board is cycling between 20 to 35 deg C.  The downward drift is repeatable and appears to be the LTZ1000A and not the DMM, however my subsequent tests show about 6 uV (slightly less) downward drift with rising temp.  I realize I'm trying to measure beyond the realistic ability of my equipment.  Its still fun non-the-less.  I do want to try and shorten the leads, but as already mentioned above I may do more harm than good.
« Last Edit: August 08, 2017, 09:46:23 pm by kj7e »
 

Offline kj7e

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Re: KX Reference
« Reply #145 on: September 08, 2017, 07:35:13 pm »
Video update on the long term project;

https://youtu.be/OIL85moSlS8
« Last Edit: September 08, 2017, 07:37:35 pm by kj7e »
 

Offline hwj-d

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Re: KX Reference
« Reply #146 on: September 09, 2017, 01:25:10 am »
You are building a very nice reference device. Thank you for sharing this.  :-+

About your TC. I've seen 10µV at the y-achsis, right? You have 0.4ppm TC at this moment. I think, that's ok?

But think about, yo're looking to your measurement system incl. your 34465a and your long measurement lines. I know, my Keysight is very sensitive to ambient room temperature too. I use preferably short cat6 twistet and shielded lines. If i touch them, it has directly impact to the measurement. Also i'm watching a direct TC change proportionate to room temperature and if i'm sitting in front of this or not.

Best regards
 

Offline kj7e

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Re: KX Reference
« Reply #147 on: September 09, 2017, 01:47:30 am »
Thank you hwj-d.

Yes, I can watch the 34465a draw sine waves with the A/C cycling.  However, I have been able to reliably duplicate the T/C drift of the my KX board. Some of this may be due to thermal EMF from the junction in the oven to the front panel  banana plugs?  In any event, I'm going to build a second KX board, this time I was a bit more careful and clean with my assembly of the SMD components and will take a bit more care with heat sinking the sensitive parts.  Ill be interested to see if one will test better or not.  If not, then I have my answer.  When I'm happy with it, I hope to send it off to someone for a better measurement than I can perform with my gear.
« Last Edit: September 09, 2017, 02:10:52 am by kj7e »
 

Offline Andreas

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Re: KX Reference
« Reply #148 on: September 09, 2017, 10:55:22 am »
If i touch them, it has directly impact to the measurement.

Is the change immediately = capacitive influence
or slowly rising / falling = thermal offset?

With best regards

Andreas
 

Offline TiN

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Re: KX Reference
« Reply #149 on: September 09, 2017, 11:12:58 am »
0.4ppm/K tempco is more than 8 times worse than expected (<0.05), so there is definately a system problem. Is your PCB version B03?  There was issue with routing on earlier B01, that affected tempco. You may want to test tempco of your 34465A to establish the measurement stability true value. Just keep LTZ ref at constant temp, and variate meter temp (e.g. insulate it in blanket with temp sensor fixed to a meter). Do it few times, and once you get the meter tempco , you can try again to measure LTZ's output tempco.

Also connections and unshielded wires can easily create more noise/offsets than tempco itself, hiding all as higher "appartent" data. Even copper-copper connection junction still have non-zero temperature coefficient.
« Last Edit: September 09, 2017, 11:21:55 am by TiN »
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Offline hwj-d

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Re: KX Reference
« Reply #150 on: September 09, 2017, 02:03:29 pm »
If i touch them, it has directly impact to the measurement.
Is the change immediately = capacitive influence
or slowly rising / falling = thermal offset?
I know, that must be kept apart.
If i touch or move them, this becomes visible at the 10 or 20µV curve at the dmm measuring with 100 plc for a time. Is it slow, or immediately?
 

Offline Andreas

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Re: KX Reference
« Reply #151 on: September 09, 2017, 02:17:45 pm »
Hello,

normally if it is thermal it will change over several 100 NPLC measurements (similar to a e-function) if you put your hand on the wiring and let it there for a while or if you remove it again. Thermal time constants are usually more in a 1 minute (or larger) range.

If it is instaneous (= within one 100 NPLC measurement) you have most likely a capacitive influence = EMI problem.

with best regards

Andreas


 
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Offline hwj-d

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Re: KX Reference
« Reply #152 on: September 09, 2017, 03:05:35 pm »
normally if it is thermal it will change over several 100 NPLC measurements (similar to a e-function) if you put your hand on the wiring and let it there for a while or if you remove it again. Thermal time constants are usually more in a 1 minute (or larger) range.

If it is instaneous (= within one 100 NPLC measurement) you have most likely a capacitive influence = EMI problem.

I know, my measurement is not optimal too. But look at this with 100 NPLC taken:


The impact at the end comes from touching [edit: carefully only DMM] using USB-Stick for screen capture just before. The new measurements after that stuck at this new level. My impression is, that this is caused from capacitive influence, but changes the measuring till other TC influence overlapped the result.

But, i think, the lm399 based 3446xa are VERY TC sensitive as others noticed too. That is not nearly comparable to the stability like a 34470a nor 3458a (... as we know ;)  )

https://www.eevblog.com/forum/metrology/mx-reference/msg1296874/#msg1296874
« Last Edit: September 09, 2017, 03:15:38 pm by hwj-d »
 

Offline hwj-d

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Re: KX Reference
« Reply #153 on: September 09, 2017, 03:32:28 pm »
Quote
0.4ppm/K tempco is more than 8 times worse than expected (<0.05), so there is definately a system problem.
Yes, but this must match high grade environmental conditions with comparable dmm's like your keithley's or 3458a's. Thats the task, after that, to have one thing in the lab, that provides this requirement, after cal, with yours and others help ...   ::)  :-+
 

Offline Dr. Frank

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Re: KX Reference
« Reply #154 on: September 09, 2017, 03:43:46 pm »
normally if it is thermal it will change over several 100 NPLC measurements (similar to a e-function) if you put your hand on the wiring and let it there for a while or if you remove it again. Thermal time constants are usually more in a 1 minute (or larger) range.

If it is instaneous (= within one 100 NPLC measurement) you have most likely a capacitive influence = EMI problem.

I know, my measurement is not optimal too. But look at this with 100 NPLC taken:


The impact at the end comes from touching [edit: carefully only DMM] using USB-Stick for screen capture just before. The new measurements after that stuck at this new level. My impression is, that this is caused from capacitive influence, but changes the measuring till other TC influence overlapped the result.

But, i think, the lm399 based 3446xa are VERY TC sensitive as others noticed too. That is not nearly comparable to the stability like a 34470a nor 3458a (... as we know ;)  )

https://www.eevblog.com/forum/metrology/mx-reference/msg1296874/#msg1296874


Well, I don't think, that the 3446x instruments are that sensitive.
Never encountered such dips, when touching the case.
I assume, that your LTZ circuit is a bit sensitive.. see current discussion about shielding, in the MX Reference thread.

To have an idea about the stability of the 34465A (LM399) vs. 34470A (LTZ1000A), see my review here:
https://www.eevblog.com/forum/testgear/keysight's-new-34465a-(6-5-digit)-and-34470a-(7-5-digit)-bench-multimeters/msg889217/#msg889217

In your graph, the scale of noise and of the dip is not obvious.
By using the scaling math function and the unit function, you might normalize your graph to read ppm deviation.. then you'd have much more resolution in the statistics also. 

Frank
« Last Edit: September 09, 2017, 03:48:52 pm by Dr. Frank »
 
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Offline d-smes

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Re: KX Reference
« Reply #155 on: September 09, 2017, 04:09:23 pm »
I know, my measurement is not optimal too. But look at this with 100 NPLC taken:


The impact at the end comes from touching [edit: carefully only DMM] using USB-Stick for screen capture just before. The new measurements after that stuck at this new level. My impression is, that this is caused from capacitive influence, but changes the measuring till other TC influence overlapped the result.

But, i think, the lm399 based 3446xa are VERY TC sensitive as others noticed too. That is not nearly comparable to the stability like a 34470a nor 3458a (... as we know ;)  )

https://www.eevblog.com/forum/metrology/mx-reference/msg1296874/#msg1296874
I agree '399 based 3446xa are very TC sensitive.  My results at https://www.eevblog.com/forum/metrology/ultra-precision-reference-ltz1000/msg1245750/#msg1245750 Dr. Frank suggested several improvements to my connections, but that didn't alter the high correlation of 34465a readings with temperature.

Regarding the reading shift from touching DMM, I too have noticed this.  I usually change grounding around and/or tie floating DUT to meter case or earth ground.  After a bit of experimenting, I can usually get the touch artifacts to go away. 
 
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Offline Andreas

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Re: KX Reference
« Reply #156 on: September 09, 2017, 04:36:43 pm »

The impact at the end comes from touching [edit: carefully only DMM] using USB-Stick for screen capture just before.

But, i think, the lm399 based 3446xa are VERY TC sensitive as others noticed too. That is not nearly comparable to the stability like a 34470a nor 3458a (... as we know ;)  )


Hello,

a capacitive effect would be reversible. So if it is a one way jump it is a different story.

From my experience the LM399 in HP devices are carefully selected (i.e. unheated tempco near zero).
If you measure the reference output voltage it should be somewhere near 6875 mV. (see LM399 thread).

with best regards

Andreas
 
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Offline hwj-d

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Re: KX Reference
« Reply #157 on: September 09, 2017, 04:37:14 pm »
Well, I don't think, that the 3446x instruments are that sensitive.
Never encountered such dips, when touching the case.
I assume, that your LTZ circuit is a bit sensitive.. see current discussion about shielding, in the MX Reference thread.

To have an idea about the stability of the 34465A (LM399) vs. 34470A (LTZ1000A), see my review here:
https://www.eevblog.com/forum/testgear/keysight's-new-34465a-(6-5-digit)-and-34470a-(7-5-digit)-bench-multimeters/msg889217/#msg889217

In your graph, the scale of noise and of the dip is not obvious.
By using the scaling math function and the unit function, you might normalize your graph to read ppm deviation.. then you'd have much more resolution in the statistics also. 

Thanks Dr. Frank for your answer. I can only learn from that, what happens (t)here.
I know, the scale of noise and of the dip is really not obvious. ;)
I don't want to mix this dip problem with that TC of my meter. That's a 34461a.

Is it right, that this meters have TC of 1ppm/k by itself? So, that we can only measure not better than that TC with it?

Best regards
 

Offline TiN

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Re: KX Reference
« Reply #158 on: September 09, 2017, 05:20:36 pm »
Quote
So, that we can only measure not better than that TC with it?
Not really. If you maintain temperature constant, you have constant tempco as well.
And since you only want to measure tempco drift of DUT, you can ignore any tempco effect on the meter's own reference completely, if it stays unchanged during complete test run. That's why I perform very slow and linear temperature ramp up and down on DUT, to make sure meter's own unstability does not introduce large errors.
If both direction ramps produce matching data, confidence is high.  ^-^
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Offline hwj-d

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Re: KX Reference
« Reply #159 on: September 09, 2017, 05:21:53 pm »
Hello Andreas,
thanks for your answer too.

Quote
If you measure the reference output voltage it should be somewhere near 6875 mV. (see LM399 thread).

I can't really do that. That meter is relative new, one year old. Maybe i put it to an other room with more constant temperature, other shielding methods, and so on.

I assume that this dip is a mistake from my own. But this relatively bad tempco is one of the meters not so good property. d-smes has confirmed this, and Ian Johnston has already dropped such a notice about this meter, as far as i can remember. Certainly it depends on the  environment, this meter must do his job.
 

Offline hwj-d

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Re: KX Reference
« Reply #160 on: September 09, 2017, 06:09:23 pm »
Quote
So, that we can only measure not better than that TC with it?
Not really. If you maintain temperature constant, you have constant tempco as well.
And since you only want to measure tempco drift of DUT, you can ignore any tempco effect on the meter's own reference completely, if it stays unchanged during complete test run. That's why I perform very slow and linear temperature ramp up and down on DUT, to make sure meter's own unstability does not introduce large errors.
If both direction ramps produce matching data, confidence is high.  ^-^
That's the problem. If i measure the DUT over the 24h and the temp changes 2-3 °C up and down, i don't know, from what the measured changes comes, maybe in combination of DMM and/or DUT, if i don't have a definitely "comparing-normal" (the objektive meta measurement) to that. So, IF i have a calibrated LTZ reference, and i know THAT TC, the deviation must come fro the dmm. And vice versa. If the LTZ is the DUT, i dont' know anything, if i can't trust the dmm. I always see the TC of the DUT AND the DMM. The LTZ-reference should control that, in the future, if it is calibrated. Maybe i'm wrong? Am I fail to see something? ;)
« Last Edit: September 09, 2017, 06:13:53 pm by hwj-d »
 

Offline TiN

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Re: KX Reference
« Reply #161 on: September 09, 2017, 06:34:38 pm »
You are correct in point that data represents total system tempco. Sure, having known "tempco" reference would make things easy.

But even without, you can still variate temperature for parts of the system (DUT only, or meter only) separately, right? :)
If your oven provides stable chamber inner temperature (<0.05C stability), you can use that easily. You just need to "anchor" one of the parts of the system to establish remaining system tempco. Having LTZ small and low power, I'd expect keeping it at stable temperature is much easier than large DMM.

If you use KX onboard MAX6610 sensors, they will allow you to check board stability well enough for the purpose. Here on page I've logged MAX6610s temperature output during my tempco test. Black ramp is reference box temperature, measured by Honeywell HEL-705 RTD. Using both sensors you can even see when LTZ oven is approaching to thermal headroom limit (closer the temperature directed from less margin from LTZ heater room). You need to stimuli LTZ DUT with much larger temperature delta, to be able even see the tempco effect, doesn't matter what meter you use, be it 34461 or 3458A, just because of the own LTZ's noise. I usually do tempco ramps from 20-25C to 40-45C to get 20C delta. If you get less than 1ppm difference, your reference good to go. :)

Said above, also means there is little meaning or usefulness in doing box tempco with just few temperature points, instead of the linear ramp, as you don't know tempco behaviour on unknown device/meter. Is it linear? Is it logarithmic? Full world of possibilities...  :scared: :bullshit:

P.S. 56K warning, linked pages are realtime JS bodge, may take a minute or two to load...
« Last Edit: September 09, 2017, 06:52:30 pm by TiN »
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Online Kleinstein

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Re: KX Reference
« Reply #162 on: September 09, 2017, 06:40:36 pm »
If one can not make the meters temperature constant, one could try to measure it and than compensate numerical. There is software to get at least linear correlation and this way get estimates for both TC's: the meter and the external reference.

 It can help if one looks at more than one temperature cycle for the external reference. However the speed of the temperature cycle is somewhat limited, as fast temperature changes can have a different effect. Not all temperature effects are instantaneous and fast changes tend to include gradients. Over many cycles variations of the meters temperature can average out, or at least a good decomposition is possible.
 
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Offline TiN

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Re: KX Reference
« Reply #163 on: September 09, 2017, 06:48:15 pm »
However the speed of the temperature cycle is somewhat limited, as fast temperature changes can have a different effect.

Yup, hence all my ramps are graceful and slow (often 40+ hours).

Linear math compensation for meter tempco during 2xLTFLU 13V reference measurement also worked well for me.
Total error was <1ppm, peaks excluded, even with 24C-31C ambient temperature change, but granted I've used bit more stable 2002.
+0.4ppm/K with reference +26.3C temp was used for linear correction.
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Offline hwj-d

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Re: KX Reference
« Reply #164 on: September 09, 2017, 07:01:54 pm »
@TiN
Ok, got it.
Then MAX6610 and your measurements is the anchor.

Thanks a lot.  :-+

Edit:
Quote
P.S. 56K warning, linked pages are realtime JS bodge, may take a minute or two to load...
Depending your upload, no problem here... ;)
« Last Edit: September 09, 2017, 07:30:30 pm by hwj-d »
 

Offline kj7e

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Re: KX Reference
« Reply #165 on: September 10, 2017, 05:48:31 pm »
Maybe the tempco is not as bad as I thought.  Repeated cycling the KX board from 25.0 deg C to 35.0 deg C four times and achieved the exact same results;
@ 25.0 deg C, 7.141510
@ 35.0 deg C, 7.141504
So 6uV over 10 Deg C, or 0.6uV/C

Scaled to 10v, that would a delta of 0.00000084 or 0.084 PPM/C.  Please correct me if I'm wrong here.
 

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Re: KX Reference
« Reply #166 on: September 10, 2017, 08:56:07 pm »
0.084 ppm/K is still slightly higher than the data-sheet value of 0.05 ppm/K, but not much. If in an environment with not so much variations, this should no be a real problem. Inside a oven environment it would be not a problem at all.
 
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Offline Mickle T.

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Re: KX Reference
« Reply #167 on: September 11, 2017, 05:36:39 am »
0.05 ppm/K is a typical value, not maximum.
 

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Re: KX Reference
« Reply #168 on: September 11, 2017, 10:58:04 am »

Thanks Dr. Frank for your answer. I can only learn from that, what happens (t)here.
I know, the scale of noise and of the dip is really not obvious. ;)
I don't want to mix this dip problem with that TC of my meter. That's a 34461a.

Is it right, that this meters have TC of 1ppm/k by itself? So, that we can only measure not better than that TC with it?

Best regards


Well, at first, the '461A and the '465A probably have the same topology of their reference around the LM399, and also the ADC circuit should be identical.
If you look into the specification, both instruments are nearly identical in DCV, without the ACAL feature of the 465A.

The 465A may have a bit more stable reference , 30ppm/yr. over 35ppm/year, due to a possibly better selected LM399.
The T.C., though, is identical, i.e. 5ppm/K. That is due to the FineLine resistor network, which is used around the reference to generate the diverse ADC reference voltages, and in the ADC itself. See 34411A schematic, which is probably identical.

The LM399 itself is specified 1ppm/k, so the '465A can autocal itself, which gives 2ppm/K. But even that is of limited use, when making T.C. measurements in strongly varying environment.

btw.: d-smes complained about the assumed bad quality and high T.C. of ´his new KS '465A, but he obviously measured 1ppm/K in his experiment, which is very good, compared to the specified 5 ppm/K. I still do not understand his criticism, one can't expect more from that class of instruments, and also I think, that the new DMMs are even better than the old 34401A.

Anyhow, it's very difficult to determine the LTZ1000s T.C. by an instrument, which is specified to have 100 times higher T.C., but it's not impossible.

At first, you may also estimate the T.C. of your '361A by means  of your LTZ1000 circuit, as d-smes has done it. As a proper designed LTZ1000 has at least < 0.1ppm/K, you would have a first guess by variation of room temperature, because the 361A is expected to have a factor of 10..50 higher T.C.
Maybe you also see 1ppm/K only, like d-smes instrument.
Your basement may offer much more stable temperatures, I achieve +/- 0.1 °C over many hours there.
So you could monitor the 361As internal temperature. I don't know if it has that parameter available over the bus. otherwise you'll have to mount a thermometer inside the instrument, and then you might be able to detect changes on the order of 0.1ppm.

If you change the LTZ1000s temperature over +/-5°C quite quickly, that would be 100 times more than the 361A, you might be able to estimate the LTZ1000 T.C.

You will notice some correlations to amount and direction of both temperature changes, so it might be possible to assign these correlations either to the 361A, or to the LTZ1000. If you have a first rough estimate of your LTZ1000 circuit, you may use it as the new baseline for further measurements.
You may also try to improve the LTZ1000s T.C. by trimming the T.C. compensation resistor.

If you are lucky to have a 2nd LTZ1000 circuit, you can bootstrap these T.C. measurements, and T.C. trimming by the same scheme as above, but your 361A would only be used for relative / ratio measurements further on.



I use my 3458A for that purpose, that may seem much easier than using a 361/365A, but it's not.
It has a (measured) T.C. of 0.5ppm/K (as specified), but that's only a factor of 2 (maybe) better than the 6 1/2 digits instrument.

I estimated my LTZ1000 circuit to have a T.C. of about 0.02 ppm/K, as that you cannot distinguish any more between both changes in temperature.
So this trimmed LTZ is at least 10 times more temperature stable than the 3458A, and will serve as the new baseline for the next LTZ circuit, I just have assembled. Goal will be to trim the next reference to ~ 0.01ppm/K, and afterwards to determine the T.C. of the first LTZ with much higher confidence.

Frank
« Last Edit: September 11, 2017, 11:42:39 am by Dr. Frank »
 
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Offline Andreas

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Re: KX Reference
« Reply #169 on: September 11, 2017, 06:56:40 pm »
0.05 ppm/K is a typical value, not maximum.

Not even a typical value.
In older data sheets: "0.05 ppm/K can be reached".
in the newest version: "0.03 ppm/K can be reached"
so it is a best case value.

Without leg length trimming and T.C. trimming I had up to 0.23 ppm/K
and was lucky to trim it down below 0.05ppm/K over 30 deg C for LTZ#3-LTZ#6.

And I fear that there is also some kind of hysteresis which limits T.C. adjustments.

Try to build several LTZ references: in the 100mV range of your DMM you can usually measure
with a factor 10 higher (noise free) resolution than in the 10V range. (as difference between 2 references)

With best regards

Andreas
« Last Edit: September 11, 2017, 07:03:43 pm by Andreas »
 
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Offline kj7e

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Re: KX Reference
« Reply #170 on: September 13, 2017, 06:08:45 pm »
I do appreciate and I'm learning from all the experts experience, advice and opinions, that of TiN, Kleinstein, Dr. Frank, Andreas, MisterDiodes and others.  Thanks Guys!

Just because no post is worth reading with out a photo, here are a few from some recent tests;

Cycling the KX board between 25.0 and 35.0 Deg C, shows 6uV swings


10 hour measurement - 100 NPLC + Math 50 reading average, KX Reference on battery power at 35.0 Deg C, 34465a at initial cal temp + or - <1 Deg C.   Less than 2uV deviation.


23 hour measurement, extension of the above 10 hour - at 12 hour mark (mid scale) I switched the KX Ref to external power which introduced a slight amount of noise that corresponds to the room A/C cycling


So as long as the room temp is somewhat stable, so is the 34465a.  It also seems the there is some merit in stabilizing the temperature environment for the LTZ1000A, at least in my case.  Also, battery power is hard to beat when it comes to noise.
« Last Edit: September 13, 2017, 06:35:52 pm by kj7e »
 
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Online IanJ

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Re: KX Reference
« Reply #171 on: September 15, 2017, 02:32:21 pm »
Hi all,

Thought I'd join in the KX build fun as I've had a couple of LTZ1000CH's sitting here since 2015........Time I did something with them!

Will build up two of them over the next few weeks. The plan is to get one of them powered up 24/7 along with one of my PDVS2's and logged via my 3458a.

Ian.
« Last Edit: September 15, 2017, 02:36:24 pm by IanJ »
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Offline hwj-d

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Re: KX Reference
« Reply #172 on: September 18, 2017, 11:49:27 am »
Regarding the reading shift from touching DMM, I too have noticed this.  I usually change grounding around and/or tie floating DUT to meter case or earth ground.  After a bit of experimenting, I can usually get the touch artifacts to go away.
In the meantime, i cut pcb grounding to DUT-case. With floating ground, i didn't got this capacitive caused dips anymore.  :)

« Last Edit: September 18, 2017, 11:56:02 am by hwj-d »
 

Offline kj7e

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Re: KX Reference
« Reply #173 on: October 05, 2017, 10:31:48 pm »
Brand new LTZ1000A showed up from Digikey today, second KX board now running.  Really took my time trying to get every part soldered in place perfectly on this one. 



Decided to place the chip 0.5mm above the board;


Going to let it burn in for a few days before I do any testing.  Running just fine at 7.161634v drawing 27mA, 15v supply.
 

Offline TiN

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Re: KX Reference
« Reply #174 on: October 11, 2017, 04:23:37 am »
Well, after all, your KX'es belong to me :)
Decided to give a helping hand to CalMachine, with his two attempts.



Obviously, my design constrains are bit unfriendly to newcomers, especially tricky SMD film capacitors.
Once I fix these two modules, I'll log them to establish stable voltage levels and send back to CM for his calibration vs their 732B standard.

That will help to also help to keep my lab calibration uncertainty as "reverse-calibration", as my last Volt calibration was done in February 2017, and is overdue.
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #175 on: October 11, 2017, 05:09:07 am »
Well, after all, your KX'es belong to me :)
Decided to give a helping hand to CalMachine, with his two attempts.



Obviously, my design constrains are bit unfriendly to newcomers, especially tricky SMD film capacitors.
Once I fix these two modules, I'll log them to establish stable voltage levels and send back to CM for his calibration vs their 732B standard.

That will help to also help to keep my lab calibration uncertainty as "reverse-calibration", as my last Volt calibration was done in February 2017, and is overdue.

I Appreciate the help and it is a great opportunity to get some international volt transfers going!

The main problem I was observing with the 1 good board was, temp co's of ~40-50 ppm/ºC.   I swapped out many components, even including the LTZ1000, and still not a working module.  My lack of building experience has got the best of me on this project.
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Offline Andreas

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Re: KX Reference
« Reply #176 on: October 11, 2017, 07:34:26 pm »
The main problem I was observing with the 1 good board was, temp co's of ~40-50 ppm/ºC.   

That should have given the hint that the heater cirquit is not working at all.

with best regards

Andreas
 

Offline TiN

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Re: KX Reference
« Reply #177 on: October 12, 2017, 12:53:25 am »
Both are fixed and logging now. I'll test tempco on weekend to see what is what. Expecting 0.2-0.3ppm/K as these are unmodified B01 PCB version. Simple trace rework should take care of that.
« Last Edit: October 12, 2017, 01:08:39 am by TiN »
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Offline TiN

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Re: KX Reference
« Reply #178 on: October 17, 2017, 05:28:39 pm »
China seller has no shame at all  :wtf: , I think world should know the "hero" with listing at Taobao. Can somebody who has account report this?  :bullshit:

Meanwhile I wrote some code to reduce experimentation setup efforts for the multiple thermal tests.
Not sure if it may be any interest for members here, but I might make in open-source project.
Currently supports K2510,K2001/K2002 and HP3458A.

Temperature curve setting:
Code: [Select]
               Peak_temp
               ______
              /      \
             | Step   \
            /          \
   Slope_pos            \ Slope_neg
          /              \
time_start Speed_pos / neg\  time_end
  ------/                  \--------- TEC temp
 Sv_start                    Sv_end
   2h     9h     2h    9h       2h

« Last Edit: October 17, 2017, 05:55:43 pm by TiN »
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Offline Zucca

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Re: KX Reference
« Reply #179 on: October 17, 2017, 10:12:46 pm »
Bastards, hope they will take it down.
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Offline ManateeMafia

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Re: KX Reference
« Reply #180 on: October 17, 2017, 11:40:23 pm »
TiN,

Sorry. You know my calibration costs are high. I have to make money somehow.  :box:
 

Offline TiN

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Re: KX Reference
« Reply #181 on: October 19, 2017, 04:29:18 am »
Maybe so, but without thermal coefficient evaluation service you have no business  :scared:  ;)

First run data on CM's KX1.

Worst case tempco calculation: -0.084 ppm/K (12 &deg;C &Delta; based on PCB MAX6610 sensor).
Best case tempco calculation: -0.039 ppm/K (19.4 &deg;C &Delta; based on TEC box sensor).

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Offline d-smes

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Re: KX Reference
« Reply #182 on: October 19, 2017, 10:30:34 am »
TiN-  It might be enlightening to dwell longer at the 20C and 40C temperatures to make sure everything fully stabilizes.  For example, between Midnight and 1 AM, voltage jumped upward while temperature was at constant 40C.

Other interesting events in the data are jumps in reference voltage with abrupt changes in ambient T and RH at 6-7:30 AM and 6-8 PM.  Reference voltage jumps down for both cases: a jump up in ambient T and RH (morning) and a jump down in T and RH (evening).

Lots to ponder.  Keep up the great work!
 

Offline TiN

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Re: KX Reference
« Reply #183 on: October 19, 2017, 11:09:42 am »
It's hard to have better stability, as essentially the meter that used to perform the measurement have same stability than the DUT, so there is no margin.
Running second time now with twice the speed and peak temperature 50C instead of 40C.
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Offline kj7e

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Re: KX Reference
« Reply #184 on: October 19, 2017, 11:55:17 am »
It's hard to have better stability, as essentially the meter that used to perform the measurement have same stability than the DUT, so there is no margin.
Running second time now with twice the speed and peak temperature 50C instead of 40C.

What temp set resistor values are being used (13K/1K) on the DUT?  It will be interesting to see it runs out of temp regulation over 40C.
 

Offline TiN

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Re: KX Reference
« Reply #185 on: October 19, 2017, 12:04:09 pm »
It's 12.5K/1K, which is about 55-57C, so there is still few degree of margin.
Current live data.

There is no much to see when LTZ's oven out of regulation, your tempco become 35-45ppm/K as result  :)
« Last Edit: October 19, 2017, 12:10:02 pm by TiN »
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Offline BFX

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Re: KX Reference
« Reply #186 on: October 28, 2017, 11:16:09 pm »
Another KX Reference is heating up to get its stability 8)




 

Offline TiN

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Re: KX Reference
« Reply #187 on: October 29, 2017, 04:42:47 pm »
BFX
Looking good.

I got the tempco data for both of CalMachine's KX references. One of which is particularly nice, showing <0.005ppm/K TC in range +34 to +43C (by box method).
Measurement setup I had covered before number of times, it's same die cast box with 40W TEC, controlled by K2510. All measurements done over 3458A in stable room temp (+/-1C), so own DMM tempco nulled out.
Except MX1 ref data, which was tested in similar box, but controlled by ILX 5910B controller instead. Meter is 3458A as well.

Data results



Legend and RAW data

1. NVS/KX1-1097 reference - this is one of my DC bank references, using KX A01 prototype PCB. 13K/1K + 120R Z202 resistors and LT1097 opamps, using LTZ1000A 2014 week 24. Board Photo. RAW data.
2. MX1-REF - this is MX1 prototype, with LTZ1000CH 2016 week 49. LT1013 + Riedon 13K/1K + 120R BMF. RAW data.
3. CalMachine's KX B01 reference unit 1 - KX B01 board, 12.5K VHP100T + 1.0K VHP103 + 120R VHP319895 + 2x80K Z201. LT2057's, LTZ1000CH 2016 week 41. RAW data.
4. CalMachine's KX B01 reference unit 2 - KX B01 board, 12.5K VHP100T + 1.0K VHP103 + 120R VHP + 2x80K Z201. LT2057's, LTZ1000CH 2016 week 41. RAW data.
5. KX B03 reference I made for member - covered in Tale 1. 13K/1K VHD200 + 120R VHP101 + 2x75K VHPs, LTZ1000CH 1990 week 15. RAW data.

MX1 reference definately needs more work, so stay tuned  :)
« Last Edit: November 01, 2017, 04:31:42 am by TiN »
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Offline BFX

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Re: KX Reference
« Reply #188 on: October 29, 2017, 05:14:48 pm »
Thx TIN but I'm curious why my LTZ is relatively cold (31.5 Celsius) ::) (I had to put some black isolation tape to LTZ of course)
I'm using 75KOhm resistors instead of 70k (for now).
Do you think its ok?
I will start some measure next year now its heating.


« Last Edit: October 29, 2017, 05:17:08 pm by BFX »
 

Offline TiN

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Re: KX Reference
« Reply #189 on: October 29, 2017, 05:18:50 pm »
If you used LTZ1000A, it's case does not get very hot. 75KOhm's are just fine, any resistor in range 65-90K are working just fine.

Is the right side zener current opamp? It should be so hot, usually it's just barely above the ambient, and heater NPN is few C warmer.
« Last Edit: October 29, 2017, 06:26:49 pm by TiN »
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Offline ManateeMafia

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Re: KX Reference
« Reply #190 on: October 29, 2017, 05:37:11 pm »
I have a second MX board that will be populated similar to the first board except I now have some of Edwin's resistors. This will help determine how much of an effect the resistors had versus the not so great layout.

The MX thread will be updated once it is up and running.

I am hoping to get some LTZ1000A from LT in the next few weeks. They are backordered but DigiKey shows a mid Nov delivery for them.
 

Offline BFX

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Re: KX Reference
« Reply #191 on: October 29, 2017, 07:14:48 pm »
If you used LTZ1000A, it's case does not get very hot. 75KOhm's are just fine, any resistor in range 65-90K are working just fine.

Is the right side zener current opamp? It should be so hot, usually it's just barely above the ambient, and heater NPN is few C warmer.

This opamp is little bit hotter but not so much (around 33.2°C ).
Do you think its too much?

« Last Edit: October 29, 2017, 07:16:42 pm by BFX »
 

Offline TiN

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Re: KX Reference
« Reply #192 on: November 01, 2017, 05:02:09 am »
I've decided to put up little index on community modules for upcoming article.  :-+



If you want to be included and have working KX module, feel free to send me photo, voltage output and used instrument, I'll add.
It's just crazy, never expected to see so much interest.
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Offline TiN

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Re: KX Reference
« Reply #193 on: November 02, 2017, 04:43:34 am »
Little sucker eated all the instrument time for a week already.
Perfectionist in me could not rest with +0.06 ppm/K tempco and parabolic-type curve on temperature extreme.



Running for a cure now..  :bullshit:

Also looks like leadtime on Digikey for LTZ1000A and LTZ1000 is now mid-december 2017/january 2018.  :scared:

« Last Edit: November 02, 2017, 04:54:55 am by TiN »
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Offline Andreas

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Re: KX Reference
« Reply #194 on: November 02, 2017, 05:32:28 am »
Hello Illya,

are you shure that you are not running out of temperature regulation above 40 deg C environment?
(which temperature setpoint?)

with best regards

Andreas
 
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Offline TiN

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Re: KX Reference
« Reply #195 on: November 02, 2017, 05:36:44 am »
Yes, I'm sure :) Setpoint is bit over 60C. You can easily see when it is running out of oven margin by very visible temperature curve. I have my old module with same setpoint, which does not show this curvy stuff and behave in nice linear way.
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Online Kleinstein

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Re: KX Reference
« Reply #196 on: November 02, 2017, 04:46:50 pm »
The TC compensation with R9 (400 K nominal) gives a curvy contribution (proportional to square root of heater power), with a stronger influence when the heater power is low. So a rather low temperature set-point or a lot of thermal insulation can contribute. With a higher temperature the contribution of R9 is expected to be linear.
The residual TC of the LTZ1000s can also vary. If too much compensation via R9 is needed the curved shape can be a problem.

Also the heater resistance has an influence - so the 400 K nominal value for R9 is an order of magnitude values only for best performance it should be individually adjusted.
 
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Offline TiN

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Re: KX Reference
« Reply #197 on: November 03, 2017, 04:19:10 am »
Kleinstein:-+
You are right on, amazing  :-DMM.

I got same guts feeling, so first thing I trimmed TC compensation resistor. Well, that ended up to be a rabbit hole. Judge youself:
Not to bloat the thread with images, I'll just add links to each run log:

* Test run 1 this is original setup, board rev.B01 , no modifications, 400K resistor. Low peak: -2.2ppm at 43C, High peak: -1.0 ppm at +55C. Worst TC box: -0.122 ppm/K.
* Test run 2 same, just faster run speed, 400K resistor. Low peak: -2.1ppm at 44C, High peak: -0.9 ppm at +55C.
* Test run 3 board rev.B01 , 226K resistor. Low peak: none, baseline, High peak: +6.0 ppm at +55C. Worst TC box: +0.194 ppm/K.
* Test run 4 board rev.B01 , 340K resistor. Low peak: -0.8 ppm at 39C, High peak: +1.75 ppm at +55C. Worst TC box: +0.055 ppm/K.
* Test run 5 board rev.B01 , 305K resistor. Low peak: -0.7 ppm at 38C, High peak: +2.2 ppm at +55C. Worst TC box: +0.064 ppm/K.
* Test run 6 board rev.B01 , trace mod to B03, same 305K resistor. Low peak: -0.4 ppm at 28C, High peak: +3.7 ppm at +55C. Worst TC box: +0.108 ppm/K.
* Test run 7 board rev.B01 > B03, 680K resistor. Low peak: -2.1 ppm at 48C, High peak: -1.4 ppm at +55C. Worst TC box: -0.066 ppm/K.
* Test run 8 board rev.B01 > B03, 470K resistor. Low peak: none, baseline, High peak: +4.0 ppm at +55C. Worst TC box: +0.117 ppm/K.
* Test run 9 board rev.B01 > B03, 563K resistor. Low peak: -0.65 ppm at 38C, High peak: +0.7 ppm at +55C. Worst TC box: -0.05 ppm/K.

FYI, each run was about 14 hours.
I think I'll settle with Run 9 results, this already sucked 120 hours of 3458A runtime.

Here's my LT1097/LTZ1000A that acted as TEC setup sanity check, no curved business.
« Last Edit: November 03, 2017, 04:51:39 am by TiN »
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Offline Andreas

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Re: KX Reference
« Reply #198 on: November 03, 2017, 06:20:54 am »
Hello Illya,

do you have really environment temperatures of 55 deg C in your lab?
I would cease work above around 30-32 deg C.

So with some safety margin I never do calibrations above ~40 deg C.

with best regards

Andreas
 

Offline TiN

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Re: KX Reference
« Reply #199 on: November 03, 2017, 11:07:03 am »
Lab temperature visible on the graph, dashed cyan line, Ambient C. It's around 27-29 this week, as I didn't do much stuff, also needed to keep it constant so I can compare run1 to run9 (3458A runs at same ACAL +/-1c span since last weekend, to avoid shifts in reading from own 3458A TC).

I never know what CalMachine's intention to use these two modules, but since he installed 12.5K resistors to get 60C setpoint, that's what I test to, minus the 5C margin room. Maybe he desire to fit one module into K2001 instead of original LM399, and "ambient" temp inside that box can reach well around +50C. Obviously since test include 20C-55C points, it's easy to process data to smaller span without any effort.

I'm done with these anyhow, and hooked HP 3458A A9 module (STD) for a spin. Let's see what she is made of.  :box:
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Offline Dr. Frank

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Re: KX Reference
« Reply #200 on: November 03, 2017, 02:04:55 pm »
BFX
... All measurements done over 3458A in stable room temp (+/-1C), so own DMM tempco nulled out....

Except MX1 ref data, which was tested in similar box, but controlled by ILX 5910B controller instead. Meter is 3458A as well.
MX1 reference definately needs more work, so stay tuned  :)

Hi Illya,

I went through your different LTZ1000 - T.C. - measurements, but maybe overlooked the decisive hint..

How do you cancel the 3458As own T.C., of about 0.5ppm/K?

If your room temperature is varying +/-1°C, then you will definitely see that variation overwhelmingly in the KX reference measurements.

The TEMP? function also deliver 1/10°C degree of resolution only, so it's quite difficult to numerically equalize temperature changes of the 3458A, when you want to measure DUTs T.C. below 0.05ppm/K.

Frank
 

Offline TiN

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Re: KX Reference
« Reply #201 on: November 03, 2017, 03:09:16 pm »
Hi Dr.Frank,

Well, hint for that is contained in my old KX datalog. You can see two runs with same config there, one with +24.2 +/-0.1C ambient temp, and second one with temperature raise to +27.2 by 3C. By using LTZ1000 output under test as a reference one can establish DMM's tempco in order of +0.1 ppm/K, so it's better than 0.5 ppm/K you mentioning.

Most of CM's KX run are with ambient temperature varied only by 0.2-0.4 C, not even full 1C. Also since we don't care about comparing absolute value from one run to another, absolute errors can be ignored.
Another confidence check is using both ramp up and ramp down curves from DUT to calculate tempco correlation. If I'd see different magnitude or output voltage not converging in the same temperatures, that would be a red flag. Of course, I would not give a guaranteed certificate on any of above listed tempco measurements, but for relative comparisons and hobby-level use I'm satisfied with numbers.

So in the end, temperature exercise on DUT is at least 70 times larger in magnitude than ambient temperature change, and meter's tempco have non-significant effect on the correlation result.
To further illustrate the point, take a look on this plot from our fellow member's lab 3458A setup. This is good example how ambient variations, like AC cycling affects LTZ DUT measurement (which is in TEC box, controlled by ILX 5910B). Yes, there is significant ~0.8ppm wobble, but you still clearly can plot a linear trend, without too much error from +2C ambient change.
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Offline TiN

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Re: KX Reference
« Reply #202 on: November 03, 2017, 04:08:25 pm »
And since you asked, here's today jem.



This is A9 STD reference, unmodified.

And updated summary LTZ tempco's, all together.

« Last Edit: November 04, 2017, 07:39:25 am by TiN »
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Offline TiN

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Re: KX Reference
« Reply #203 on: November 04, 2017, 06:24:49 am »
Since Andreas asked, here is how it looks like when LTZ reference is out of oven thermal margin:



I'm testing two references with zeners in sockets, same TEC box, two meters.
« Last Edit: November 04, 2017, 08:36:25 am by TiN »
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Offline Dr. Frank

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Re: KX Reference
« Reply #204 on: November 04, 2017, 07:30:52 am »
And since you asked, here's today jem.



This is A9 STD reference, unmodified. Single digit ppb/K tempco till +47C box temperature !

And updated summary LTZ tempco's, all together.

Sorry Illya,

but I suppose, that you have a fundamental bug in your calculus of the T.C.

You obviously want to calculate the T.C. each 1°C step, by calculating the derivative delta(U)/delta(T), where delta(U) is the change of the reference voltage over 1°C, already expressed in ppm of this reference voltage, as this is already divided by the baseline reference voltage, and delta (T) is the change of the temperature, that is identical to 1°C.

So, the column 'ppm dev' already gives your 'momentary' T.C. value, but in your column 'T.C.' you again (for the second time) divide by the reference voltage 7.184V, which gives insanely small values, because of the quadratic division in Uref.

I also see a numerical problems with your calculus of the T.C., as the measurement of the reference voltage has a typical standard deviation, or reference rms noise of 0.02 .. 0.04ppm already, if you measure at NPLC100.
This noise is not reflected at all in your T.C. curves; they look smooth as a babys butt.. which should you also make you think, that something is fishy here..   :-//

For sure, your measurements of simply Uref over T look exactly like mine, that is with a lot of overlayed noise, and then you would have to use a reasonable smoothing algorithm, or a graphical method, i.e. box method, to get the correct T.C. numbers, or function of T.C. over temperature.

Regarding the T.C. of your 3458A, it would be great if it would really have 0.1ppm/K, but I would also like to see a reliable and solid measurement, assuring that parameter.
 
Frank

« Last Edit: November 04, 2017, 07:33:18 am by Dr. Frank »
 
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Offline TiN

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Re: KX Reference
« Reply #205 on: November 04, 2017, 08:24:50 am »
Aha, I hear what you saying now. Perhaps I got over-excited there a bit, and got too much zeros.

I acknowledge this calculation topic have icebergs under, perhaps good time to establish common definition to avoid further confusion?

Here's same plot, with actual every data point over the temperature.



Dashed line is step approximation fit, which is not subjected to noise and smooth.
Here also see typical 0.1ppm-ish noise derived from 3458 & DUT.

Is all this look right?

On second part, 3458 tempco, it's great time now, so I'll stabilize temperature of the DUT (2 x LTZ1000) at let's say +24.000 +/-0.005C and variate ambient temperature from current +28 to +22. That should give us 6C of 3458A temperature change to estimate DMM TC?
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Offline Dr. Frank

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Re: KX Reference
« Reply #206 on: November 04, 2017, 01:21:32 pm »
Illya,

that all looks much more reasonable and solid.
Anyhow, now one can really see the good quality of your measurements, in relation to the reference noise.


I don't know, where to find an official definition of this 'box method'.
 
As implemented by Vishay for the determination of the T.C. of their resistors, they probably use 3 temperature points only, like -55°C, +25°C and +125°C.
Their German representative once measured my VHP202 at 25, 60, 100 and 125°C only, and calculated the average T.C. between these points.

G.R. measured the new 120 Ohm resistor samples between: 23=> 35 =>45 => 35 => 23°C.
They let the DUTs settle for about 24h at each single point, before they take the measurement.
However, they got totally puzzled values, even with different signs for the T.C., and that was due to this big hysteresis of this special value.


Therefore, our method of continuously measuring the reference voltage en passant, i.e. while the temperature slowly changes, and then to draw a box around the horizontal and vertical limits of the measured graph, gives much better and more information about the DUT.
You only have to take care, that not too big a hysteresis or shift occurs, which often happens, when the temperature is changed too fast.
In a physical sense, the measurements have to be made in or near the 'equilibrium state'.. and it's always a problem to identify this correctly.

This box method is a kind of averaging, and necessary only, when a non-linear or hysteretic behaviour is present.

Yep, if you were able to change the temperature of your 3458A by 5°C, you'll get a real good measurement of its T.C. for DCV, w/o ACAL.
I assume, the root cause of this T.C. is located mainly in the A/D ASIC, i.e. these internal gain resistors, which you were very familiar with, I think  :-DD
This famous cal constant 72, related also to the AN18 stability problem, should directly depend on the environmental temperature (which is not considered in the AN18).
What do you think?

I have measured this CAL? 72 regularly, but could not find a real drift over time (fortunately), but a negative dependency over temperature (TEMP? CAL? 175), of about -0.3ppm/°C.
The graph over temperature has a lot of scatter, because the temperature sensor is on the opposite site than the A/D board.
But these -0.3ppm/°C are in good accordance with the DCV T.C. of +0.4ppm/°C, which my wife measured for my 3458A..
The difference in value might to be explained by the T.C. of the internal LTZ1000A  reference.

Frank

« Last Edit: November 04, 2017, 02:12:36 pm by Dr. Frank »
 

Offline TiN

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Re: KX Reference
« Reply #207 on: November 04, 2017, 01:39:51 pm »
Yes, hysteresis is the reason why I use slow ramp up/down for all TC data collection, instead of step gaps.
With Raspberry Pi and GPIB it's all easy to program.

For meter tempco data, be my guest : https://xdevs.com/kx56_test2_tc/
It's current live log. I'll leave it running as low as room AC can go.

Beginning of the graph is with ambient temp +29c (cyan dotted line)
TEMP? readings from both meters are bold blue/violet. One of my meters does not have A1 shield inside, hence RAW TEMP? data is offset by 4.9c. External covers are all on.
DUT reference are two LTZ modules, in own TEC box, controlled at +24C +/-0.02C peak (black is TEC box sensor temp, thermistor YSI 44006).
RAW CSV-datafile is in link under graph as well.

From what I can see - DCV 10V tempco is un-measureable here (<0.1ppm/K). Even if I take worst peak-peak 0.5ppm (dots are individual samples, lines are average) and divide by current TEMP? change (42C -> 38C = 5C) that gives 0.1ppm/K for blue meter. Second "B, green" meter shows only noise, no tempco.

If meter own TC would be 0.1ppm/K, then output reading should be already off by 0.5ppm, which is clearly not the case, if we go by averaged "noise-free" values.

For reference, if that worth anything, "blue" meter has new A3 Keysight ADC made in 2016, bought year ago, "green" meter has A3 Agilent ADC, made in 2004.
« Last Edit: November 04, 2017, 01:56:30 pm by TiN »
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Offline Dr. Frank

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Re: KX Reference
« Reply #208 on: November 04, 2017, 01:54:15 pm »
By the way, I think it's instructive to refer to this old NBS Technical Note 1239, about the performance of solid state voltage references:
https://archive.org/details/solidstatevoltag1239fiel

In Design / Performance Goal P4, a T.C. of < 0.01ppm/K is recommended, which obviously none of the commercial references achieves..

A description, how to correctly measure and display that T.C., is also not available.

Frank
 

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Re: KX Reference
« Reply #209 on: November 04, 2017, 02:03:42 pm »
Wow, both your 3458A are really impressive!
Their T.C.s are practically zero.
But it's really hot, where you live.

 

Offline TiN

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Re: KX Reference
« Reply #210 on: November 04, 2017, 05:18:37 pm »
Outdoor temp today in here north of Taiwan is around +18C. I just had cold last week, so I did not turn on AC last week or so.
I don't have luxury of basement as of yet, it's apartment on 10th floor, with gear running 24/7, so ambient temps easy to climb 28-30c without aircon permanently on.

I think we saw enough on 3458A's tempco question, time to test some other's  :)
3458A Green = +0.048 ppm/K 10V TC (0.36 ppm with 7.4C drop).
3458A Blue = +0.06 ppm/K 10V TC (0.45 ppm with same drop).
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Offline bopcph

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Re: KX Reference
« Reply #211 on: November 08, 2017, 03:41:27 am »
@CalMachine

If you could get a smaller dome to fit a few mm inside the one you are using now.
You would create a dobb. wall dome decreasing the heat transfer thru the dome(s) and thereby also reducing the risc of turbulence/convection.

Drilling away the free areas around the LTZ, inside the guard-ring reduces the mass of FR4 material, it should make it easier for the LTZ to get the mass in equilibrium - just a guess :-)
« Last Edit: November 08, 2017, 03:57:27 am by bopcph »
 

Offline TiN

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Re: KX Reference
« Reply #212 on: November 08, 2017, 04:10:49 am »
Tested good old jumpy ACH. Funny enough, other than jumps it's fine ref.
It's reference of 0.6 ppm jumps. :D.

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Offline MK

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Re: KX Reference
« Reply #213 on: November 08, 2017, 06:33:16 am »
with the jumpy ACH perhaps you could try a set of different currents, at a bit higher current those jumps may go away?
 

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Re: KX Reference
« Reply #214 on: November 30, 2017, 01:27:35 am »
Chasing Zero's and accuracy/stability is addictive  :scared:

Boards ordered. If anyone in Oz is interested I am going to keep two but one will be available for cost.

Now off to arrange components  :)

Freaky stable untrimmed Max6350 @ 21 C but I "NEED" more   8)
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Offline kj7e

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Re: KX Reference
« Reply #215 on: December 09, 2017, 12:11:32 am »
I was not entirely happy with the tempco of my KX reference with the LTZ1000A, it wasn't that bad, but I felt it should have been better.  The best I could test with a 34465A was about 0.08 to 0.1 ppm/K.  Since I had the A version I did as the data sheet said and omitted the 400K tempco resistor.  Just as an experiment I added the tempco resistor starting with 1M Ohm, then 680K, 470K and 300K.  Each time seeing an improvement and finally seeing a nearly flat tempco with 300K.   I even tried 270K and 330K but found the sweet spot at 300K, what a difference! I cant say how pleased I am now.  Since that time, I've added a Keithley DMM7510 and I'm able to further verify my findings.  Here is some data from a 15 Deg C to 35 Deg C temp sweep;

The meter was null'd when the reference temp was 15 Deg C in order to easily see the uV deviation.  The bump about mid scale is where I powered on the oven to continue warming from about 25 Deg C to 35 Deg C;




Zoomed in to show some of the noise and individual data points;


So there is about a 3uV (-1 to +2) change across the sweep, this was repeated about 5 times with the same results. 3uV = 0.42 ppm / 20 Deg sweep = 0.021 ppm/K.

This is on the second KX board I built, the first one (which had a better initial tempco) also improved significantly but sweet spot was 390K.
« Last Edit: December 09, 2017, 12:26:48 am by kj7e »
 
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Offline TiN

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Re: KX Reference
« Reply #216 on: December 14, 2017, 04:26:10 am »
Alright, both CalMachine's references are now repaired, tested, tweaked and ready to be shipped tomorrow.

I've packaged them into metal enclosures, with Low Thermal binding posts for outputs and regular binding posts for input power.
Final calibration test data and tempco plots for module 2:



 :)

And time scale plot of the same data set.

Red here is module 1 measured in ambient air, using K2002, powered by VRLA battery.
Green and blue is module 2, on 3458s, measured with 18-50c ramps in TEC box chamber.

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Offline Pipelie

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Re: KX Reference
« Reply #217 on: December 14, 2017, 06:29:33 am »
TiN
Well done on your TC trim.  :-+
I got some data, would like to share.
test gear:
1.HP3458A
2.DIY 16 channel scanner
I always use scanner for TC test, and some times need my DIY thermostatic chamber. 

« Last Edit: December 14, 2017, 06:33:48 am by Pipelie »
 
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Offline TiN

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Re: KX Reference
« Reply #218 on: December 14, 2017, 11:20:42 am »
It seems like Mr. CalMachine does not want to give me shipping info at ticket 119 in time, so these two little boxes will go out tomorrow to person, who gives shipping info.  :scared:

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Offline pitagoras

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Re: KX Reference
« Reply #219 on: December 14, 2017, 11:55:31 am »
PM sent
 
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Offline Pipelie

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Re: KX Reference
« Reply #220 on: December 14, 2017, 12:55:20 pm »
Hello TiN,
Did you test the Voltage Noise of LTZ1000 and 10V ?
I think it would be useful and interesting data  worth of collection.
the TC of LTZ1000 could be trim in most case,but noise performance is hard to improve. 
here are the noise performance of my three 732a:
1.  2uVpp,
2.  1.6uVpp
3.  1uVpp
and the noise of LTZ are various too.
 
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Offline Dr. Frank

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Re: KX Reference
« Reply #221 on: December 14, 2017, 02:36:53 pm »
Hello TiN,
Did you test the Voltage Noise of LTZ1000 and 10V ?
I think it would be useful and interesting data  worth of collection.
the TC of LTZ1000 could be trim in most case,but noise performance is hard to improve. 
here are the noise performance of my three 732a:
1.  2uVpp,
2.  1.6uVpp
3.  1uVpp
and the noise of LTZ are various too.

What is the time constant, over which you determined these noise numbers?
on the order of seconds to minutes, you may get the basic zener noise, when you have 1h, for example, you will also measure some popcorn noise .. Allan deviation is probably the best way.. and I did not see such for 732A / 732B, yet.
Would be quite interesting

Frank
 

Offline Pipelie

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Re: KX Reference
« Reply #222 on: December 15, 2017, 01:59:03 am »
Hi Dr. Frank,
I use my DIY 0.1-10Hz   low frequency noise meter to test the noise of voltage reference.
I‘av build more than 35 unit for a group-buy, here is what it looks like.
https://www.eevblog.com/forum/metrology/diy-low-frenquency-noise-meter/50/     Reply #68 by zlymex.

and some test result, hope this data could answer your question.
PS. I don't have the suitable equipment to record the output of noise meter for an hour or so.
 
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Online beanflying

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Re: KX Reference
« Reply #223 on: December 28, 2017, 01:21:38 am »
Santa arrived late and he forgot my LTZ's and Vishay's. Maybe I wad a bit naughty  ::)

Hurray up and wait some more .....
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Offline kj7e

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Re: KX Reference
« Reply #224 on: January 04, 2018, 03:34:45 am »
Finally installed my first KX board in a proper enclosure, used a Hammond 1590B with some Pomona 3770 binding posts on the output and 3760's for the input.

Sorry, the photo orientation seems to be amiss.







The board is recessed in the foam, only the edge of the board makes contact with the foam surrounding;


The foam on the lid then compresses to gently sandwich in the board in the recessed area;


This seems to work very well and should not present any stress on the board as well as add some thermal insulation to minimize external temperature effects.
« Last Edit: January 04, 2018, 03:57:19 pm by kj7e »
 
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Offline kj7e

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Re: KX Reference
« Reply #225 on: January 04, 2018, 07:10:38 pm »
Using one of Pipelie's LNA noise meters, here are some noise measurements comparing the LTZ1000 KX #1 in the Hammond enclosure above, vs the PDVS2 (LM399 based) at 7.14150v.

The LNA has a gain of 10,000, all measurement @ 10mV/div for 1uV/div.

Baseline LNA + scope noise, 280nV p-p;


LTZ1000 over 14 seconds, 1.12uV p-p;


LTZ1000 over 140 seconds, 1.256uV p-p;


So right on the money with the data sheet spec of ~ 1.2uV p-p.

LM399 based PDVS2 over 14 seconds, 6.04uV p-p;


LM399 based PDVS2 over 140 seconds, 5.68uV p-p;


« Last Edit: January 04, 2018, 09:49:14 pm by kj7e »
 
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Offline AG7CK

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Re: KX Reference
« Reply #226 on: January 04, 2018, 11:03:02 pm »
A very telling post. Thanks.
 

Offline Pipelie

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Re: KX Reference
« Reply #227 on: January 05, 2018, 01:55:35 am »
Thank you! kj7e

Finally , I find a supply for the  Hammond 1590B in local, Thanks for kj7e who provide the part number of the case.

nice work on the black Insulation materials,How did you do that? it looks perfect fit in the case.

use a Coaxial cable to connect the reference and LNA, will get a little better result.

here is some of my test result.
« Last Edit: January 05, 2018, 02:07:44 am by Pipelie »
 
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Offline kj7e

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Re: KX Reference
« Reply #228 on: January 05, 2018, 02:04:38 am »
Thank you! kj7e

Finally , I find a supply for the  Hammond 1590B in local, Thanks for kj7e who provide the part number of the case.

nice work on the black Insulation materials,How did you do that? it looks perfect fit in the case.

use a Coaxial cable to connect the reference and LNA, will get a little better result.

here is some of my test result.

Fresh razor blade, ruler, Dremel tool and a steady hand  :)

Those where taken with coaxial cables and a dual banana to BNC adapter on the LTZ1000 box.  The LM399 based reference is about where it should be as its much more than a bare reference, there is a 10v buffer, DAC and other circuitry and another output buffer, so lots of things going on there to add a bit of noise.  The LTZ1000A is about where it should be but I have two other KX boards to test.  Ill compare all three soon and see if how they stack up.
« Last Edit: January 05, 2018, 02:10:28 am by kj7e »
 

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Re: KX Reference
« Reply #229 on: January 17, 2018, 04:03:01 am »
Some additional noise measurements from my latest KX (#3 with LTZ1000A date code 1750).

The test setup;


Baseline LNA/scope noise, 260nV;


14 seconds, 960nV;


140 seconds, 1.3uV;


Found some very interesting things regarding ground loops and my gear with this noise meter, very handy indeed.

 
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #230 on: March 03, 2018, 04:00:16 pm »
I've got some measurement results of my 2 KX modules.  Dubbed 'KXBlue' and 'KXGreen' from the label TiN_MaN placed on them.

More tests will be run in the future.  KXBlue had a few ACAL incidents during its ramp, makes it not look so stable.  Here, the TC of the measurement system realllllly pokes through  :popcorn:
All your volts are belong to me
 
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Offline Mr. Scram

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Re: KX Reference
« Reply #231 on: March 06, 2018, 08:55:29 am »
Forgive me my ignorance, but I seem too see a lot of different references and I think most or all are based on the same reference IC. What is the idea behind these variations? Are they attempts to achieve the same thing or do they have differentiated purposes?
 

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Re: KX Reference
« Reply #232 on: March 06, 2018, 10:59:15 am »
...
Are they attempts to achieve the same thing ... ?

Yes, the ltz1000 and all around is fun!  ;D

 

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Re: KX Reference
« Reply #233 on: March 07, 2018, 11:55:13 am »
... and don't forget this little boy or girl inside all of us, who/she allows to be creative all over the lifetime ;)
 

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Re: KX Reference
« Reply #234 on: April 10, 2018, 07:47:17 am »
I jumped on the KX train!

I picked up a yard of 100% wool, and cut out a small piece to place between the LTZ and the board, to disrupt air drafts.  Hopefully the wool will be durable enough to be a long-term solution (it is a solid sheet of wool which I poked the leads through before soldering in the LTZ, so it is now permanently part of the build).

I went with hermetic resistors, as this ref will be (eventually) traveling to Taiwan to fetch the TiN Volt.  Hopefully they will minimize any travel-related offsets (e.g. regional humidity differences).

I threaded a 1N5819 schottky into the positive input, for reverse bias protection.

My surface mount soldering is pretty horrific, but it got the job done :)  C1, 2, 3, and 9 gave me particular trouble -- it felt like I was installing a 1206 part onto an 0805 pad.

Edit: wow, you can get an 8"x8" square of wool for $3 https://www.birdbraindesigns.net/wool-black
« Last Edit: April 10, 2018, 08:03:42 am by cellularmitosis »
LTZs: KX FX MX CX PX Frank A9 QX
 
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Offline CalMachineTopic starter

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Re: KX Reference
« Reply #235 on: January 30, 2019, 12:14:30 am »
It's been a little over a year since my 2 KX modules made the journey across the Pacific Ocean to TW. 

With the advent of surpassing the year mark, I'd like to share my current results  :-+

KX "Blue"




KX "Green"


All your volts are belong to me
 
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Offline TiN

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Re: KX Reference
« Reply #236 on: March 02, 2019, 10:55:53 am »
That moment, when you get YT ads showing your PCB design, while watching EEVBlog video...



Not to mention stolen video content from Marco Reps  :-- 
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Offline syau

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Re: KX Reference
« Reply #237 on: March 03, 2019, 01:39:09 am »
That moment, when you get YT ads showing your PCB design, while watching EEVBlog video...



Not to mention stolen video content from Marco Reps  :--

 :palm:
 

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Re: KX Reference
« Reply #238 on: March 03, 2019, 02:16:09 am »
Sux a lot. Have you and Marco tried to copyright strike them or get together with others who seem to have had their designs and videos 'borrowed' for their commercial gain? All us other viewers is give them a dislike or when they leave it available give them a serve in the comments section.

Not that they have a large youtube following but they do have a lot of paid and sponsored noise out there on youtube from content creators.

Code: [Select]
https://www.youtube.com/watch?v=dVEY3BxgHNA
Code: [Select]
https://www.youtube.com/watch?v=1FJXEL3Ff4Q
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Offline grizewald

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Re: KX Reference
« Reply #239 on: March 31, 2020, 10:49:22 am »
People are still making KX references. Well, I am at least.  :)

As my Test Equipment Addiction has grown, I found myself needing better DC references when I bought my first 7.5 digit multimeter. Having read so much about the LTZ1000 and TiN's KX reference project here on the forum, I decided to build some! I have built two so far and used the project at OSHPark by SvanGool for the PCBs, so I might end up building a third. The BOM is as per the very helpful BOM on xDevs.com and I have used LTZ1000A reference ICs for both builds.

A big thanks to TiN for making this project available to everyone!

Reference number one was a bit of a learning experience as it was my first project with surface mount components. I think it turned out fairly well. I even managed to avoid the traps presented by the various guard traces!



Of course, getting hold of the right resistors for an LTZ1000 reference is a challenge, but between Mouser and my favourite Polish eBay seller, I procured the following resistor set for reference #1.

R5 = Vishay RCK02 12.2955K 0.01% 5ppm
R4 = Vishay S102 1K 0.01% 2ppm   
R3 = Vishay Z201 120R 0.01% 0.2ppm
R6 = Vishay RCK02 68.1K 0.01% 5ppm 
R7 = Vishay RCK02 68.1K 0.01% 5ppm

I think 12.29K actually turned out to be a bit low for R5, so I'll probably be replacing that with a 13K resistor instead.

Having got reference #1 nicely boxed up and discovering how useful it is to put the wires through the plastic frames which hold the end plates of the Hammond case before soldering the wires to the connectors  :palm:



I made a second parts order to start building reference #2. This time, I chose a slightly different resistor set with better stability.

R5 = Vishay S102 13K 1% 2ppm
R4 = Vishay Z201 1K 0.01% 0.2ppm   
R3 = Vishay S102 120R 0.01% 2ppm
R6 = Vishay RS92NA 75K 0.1% 2ppm 
R7 = Vishay RS92NA 75K 0.1% 2ppm 

Here is reference #2, all cleaned and waiting for the LTZ1000 and precision resistors to be installed. I skipped the pin headers this time as they don't really provide any benefit once the reference is cased.



Finally, I had reference #1 cased and had also acquired an Agilent 34401A. It seems to agree very nicely with the reference which is impressive for a multimeter which has not been adjusted since its original factory calibration some 20 years ago!

In the background of the shot is reference #2 which now has the resistors and LTZ1000 installed and is being made ready for installation in its case. The precision resistors are quite high off the board because they don't match the spacing of the holes in the PCB and I didn't want to bend the leads too close to the resistors' package. Both references have a foam ring to keep the legs of the LTZ1000 nice and cosy on top of the board and both also have a foam disc underneath the PCB to keep convection disturbances to a minimum there as well.



Both references are now being burned in and have been on constantly for about ten days now. Reference #1 is drifting slowly downwards whereas reference #2 seems to be very stable from the start. Once both references have been powered for at least a month, I'll start logging some long term data, but I noticed something strange in the data which I have already captured.

Below are two plots, one taken on my rather noisy Solartron 7061 and the other (which is currently running) from the 34401A.

(The marked downwards trend, followed by a recovery near the end of the first plot is due to me experimenting with the drift compensation feature on the 7061. Just at the end of the plot, I manually initiated a drift correction. The voltage recovers almost to the original level, but not quite and further testing with reference #1 shows that it's still slowly drifting down, hence why I think I'll swap out R5 for a 13K resistor.)





The common feature here which is puzzling me is the occasional negative going 'pop' from both references. Is this normal during the initial settling in period?

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Offline Dr. Frank

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Re: KX Reference
« Reply #240 on: March 31, 2020, 11:10:39 am »
These downward spikes are typical for the original schematic, which probably picks up any external disturbance. 
These may last several seconds, or several samples, then it's a sign that the oven control being disturbed, if it's only a single point each, then this might be disturbance of the 34401A input only.
Therefore that has nothing to do with settling, this will be a permanent effect.

Check your PSU, if it's possible to shield it, or add a ferrite ring.

Other circuits (from Andreas) greatly suppress these spikes, maybe you go back into the history of this famous "Ultra Precision Reference LTZ1000" thread, where this was demonstrated several times.

This 12.2955K resistor is fine, gives about 55..60°C oven temperature. You should determine this on your own, using your 34401A. Method is described also deeply back in this thread.

Btw: If you encounter longer dips, lasting for many minutes, hours or days, TiN himself called that 'jumpy reference', then this would be caused by the A version itself.
Some samples show these jumps, due to not completely annealed die cast.

Frank   
« Last Edit: March 31, 2020, 12:38:10 pm by Dr. Frank »
 
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Online Kleinstein

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Re: KX Reference
« Reply #241 on: March 31, 2020, 12:46:31 pm »
The measurements with a DMM are only as good as the DMM. So with the 34401 and Solatron 7061 one would see more of an effect of there reference (LM399 and likely 1N829). The large spikes are more like an external problem.
 

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Re: KX Reference
« Reply #242 on: March 31, 2020, 03:34:10 pm »
The measurements with a DMM are only as good as the DMM. So with the 34401 and Solatron 7061 one would see more of an effect of there reference (LM399 and likely 1N829). The large spikes are more like an external problem.
@Klenstein is so right and I found this out myself.  It started with my 34401A measuring precision voltage reference which eventually led me to the 3458A.  Better voltage reference requires a better DMM and so the tug of war goes!  Then you end up like some others here and need 4 or 5 different 8.5 digit MM which, of course, requires more precision references.  And with all the 3458A's you need a better resistance standard.  That's how it goes: 

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Offline grizewald

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Re: KX Reference
« Reply #243 on: March 31, 2020, 04:49:46 pm »
Thank you for the replies gentlemen.

I'm fully aware that the meters I own have references far inferior to the LTZ1000, but that doesn't reduce the usefulness of the KX references to me. Quite the opposite in fact as the KX reference is capable of showing up problems on the meter itself and I can still get a good impression of how stable the references are after burn in with my inferior meters. This should let me choose a good time to post them to a friendly cal lab or fellow volt nut for characterisation.

I'm still looking for a proper metrology grade meter and was in the running for a Datron 1281 yesterday, but the bidding quickly passed the limit of my test gear fund in the remaining few minutes of the auction. So for now, I'll have to make do with what I have.

When I first saw these excursions on the 7061, I immediately suspected the meter, but seeing them appear when using the other reference on the 34401A, I began to wonder if it was specific to the KX reference itself.

They are both being run at 12V from a Thurlby PL320 linear lab supply, so the power is quiet and stable.

I looked through the reference #2 log and found the three samples with large negative jumps and indeed just one sample is involved, just as the single line thickness on the plots would imply:

Code: [Select]
2020-03-30 23:46:44,24.90,30.28,1029.25,+7.11377860E+00
2020-03-30 23:46:46,24.90,30.28,1029.25,+7.11371180E+00
2020-03-30 23:46:48,24.89,30.29,1029.26,+7.11377920E+00

as is the big jump of 20ppm:
Code: [Select]
2020-03-31 00:07:38,24.86,30.41,1029.22,+7.11377630E+00
2020-03-31 00:07:40,24.86,30.41,1029.22,+7.11363070E+00
2020-03-31 00:07:42,24.86,30.41,1029.22,+7.11377340E+00

and the third blip at just after 00:30

Code: [Select]
2020-03-31 00:35:35,24.76,30.65,1029.10,+7.11377550E+00
2020-03-31 00:35:37,24.76,30.65,1029.10,+7.11369950E+00
2020-03-31 00:35:39,24.76,30.65,1029.10,+7.11377570E+00

The two spikes on the 7061 log from reference #1 are similar, just one sample blips, one just before midnight and one just after:

Code: [Select]
2020-03-22 23:48:20,25.52,31.14,1039.00,+7.134534
2020-03-22 23:48:36,25.52,31.14,1039.00,+7.134428
2020-03-22 23:48:52,25.52,31.14,1039.00,+7.134538


2020-03-23 00:04:06,25.27,31.40,1038.94,+7.134537
2020-03-23 00:04:22,25.27,31.40,1038.94,+7.134497
2020-03-23 00:04:38,25.27,31.40,1038.94,+7.134535

I also saw a line at just after midnight in the reference #2 log with a problem caused by my logging system where the script seems to have been updating the environmental data at the same time it was being copied to the new line in the log file resulting in missing fields between the time and voltage columns. (The script runs multiple background processes.) Oddly, gnuplot doesn't complain about the empty columns when it processes the file.

Code: [Select]
2020-03-31 00:09:57,24.89,30.51,1029.26,+7.11377890E+00
2020-03-31 00:09:59,,+7.11377990E+00
2020-03-31 00:10:02,24.92,30.51,1029.28,+7.11377880E+00

So I'll need to fix things so that can't happen again!

From this, I'd infer that the reference chips are thankfully not one of TiN's "little jumpers".

The reference that is currently connected to the 34401A is not using the leads in the picture. It is connected with a twisted pair of PTFE insulated silver plated copper wire with low thermal EMF spades on the reference end and Stäubli low mass banana plugs on the meter end. The reference connected to the 7061 would have been connected with the original Solartron measurement cable - also very high quality and shielded.

The only local interference source I can think of is my temperature/humidity/pressure sensor which is sitting on the desk near the reference under test in each case. This sensor reports back to a local MQTT server wirelessly, so there's a 2.4GHz wireless transceiver close by operating for a very short time every minute as the sensor publishes the latest readings.

I can imagine that transmission being capable of causing a disturbance, but with the 34401A returning a new reading every two seconds, I'd expect the disturbances to affect the result much more often than just two readings out of the nearly 41000 that there are currently in the log. I'd also expect the disturbance to have an equal possibility of generating a positive or negative going disturbance and I've never seen a positive one.

To attempt to see if that is the cause anyway, I'll move the sensor a few metres away from the desk and see if I have any ferrites to put on the power leads from the Thurlby supply. The temperature is fairly constant in my apartment, so moving the sensor away from the bench shouldn't affect the relevance of the data to any significant degree. At least it won't get caught by the morning sun as it did today, resulting in the temperature spike at around 08:00 before I shut the blinds on the windows.

edit: The line with the missing columns was not responsible for the largest 20ppm jump. My mistake.
« Last Edit: March 31, 2020, 08:37:37 pm by grizewald »
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Online Kleinstein

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Re: KX Reference
« Reply #244 on: March 31, 2020, 05:16:38 pm »
The LM399 reference in the 34401 can by tricky with random jumps from a kind of popcorn noise. So it can appear perfectly stable for minutes and than suddenly just a few µV. A little like TIN little jumper. The only good thing with a well aged 34401 is that there would not be much normal drift with time. Here a new LTZ1000 may actually be inferior. It is still tricky with possible low frequency noise.

About the only way to really judge the reference better than the meter is to use both LTZ1000 refs and use the meter to measure the difference only.

The jumps just a round midnight are somewhat suspicious. One rather strong EMI source are mobile phones. From time to time they send a really strong  (e.g. full power) sync / station search pulse / command (a few seconds, maybe repeated a few times). This may happen just around midnight. 
 

Offline grizewald

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Re: KX Reference
« Reply #245 on: March 31, 2020, 05:38:52 pm »
The jumps just a round midnight are somewhat suspicious. One rather strong EMI source are mobile phones. From time to time they send a really strong  (e.g. full power) sync / station search pulse / command (a few seconds, maybe repeated a few times). This may happen just around midnight.

That's a very interesting point and I know you've been investigating RFI recently.

I'll make sure to keep my mobile in another room this evening and see if there are any disturbances tonight. I'll be leaving this particular log running for a few more days, so I may have the opportunity to see if there is any correlation. It also just occurred to me that my daughter's bedroom is just behind the bench on the other side of the wall where my bench is. That particular wall is a load bearing wall and is made from concrete and rebar, but I can't imagine the rebar having any effect on such high frequency signals.
 
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Offline grizewald

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Re: KX Reference
« Reply #246 on: March 31, 2020, 09:22:18 pm »
I just went back and edited my post from 17:49. It turned out that the -20ppm jump was for real. My mistake.

Reflecting on the discussion so far, I'm finding it very hard to reconcile either popcorn noise in the meters' references or EMI with this problem as I just can't see why it would always result in a negative going spike and never a positive one. Maybe there's something specific about the length of a PCB trace on a specific node in the reference circuit making it act as a perfect antenna for a specific frequency and always manifesting as a negative going spike.  :-//

I'll carry on trying to eliminate possibilities.
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Offline Dr. Frank

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Re: KX Reference
« Reply #247 on: March 31, 2020, 11:21:20 pm »
I just went back and edited my post from 17:49. It turned out that the -20ppm jump was for real. My mistake.

Reflecting on the discussion so far, I'm finding it very hard to reconcile either popcorn noise in the meters' references or EMI with this problem as I just can't see why it would always result in a negative going spike and never a positive one. Maybe there's something specific about the length of a PCB trace on a specific node in the reference circuit making it act as a perfect antenna for a specific frequency and always manifesting as a negative going spike.  :-//

I'll carry on trying to eliminate possibilities.

Excuse me,
I think that I have given you the correct hints, as I have seen exactly the same effects (negative dips) either with my 34401A, over 15 years ago (yes, I was probably one of the first amateurs to build two LTZ1000 circuits), I also observed always negative glitches and these were on the order of -1..5ppm, sometimes bigger. Later on, about 10 years ago, with my then freshly bought 3458A, I saw exactly the same glitches, maybe less, beacuse in the meantime I made some improvements on the (linear) power supply. Hopefully, you're not using a cheapo SMPSU ?

The better reference of the 3458A makes things easier, i.e. less noisy and more stable (relative to each other), but the essential characteristics can very well be extracted with a 34401Al, please take Andreas as an example. Thesed glitches you have observed, have absolutely nothing to do with the quality of your 34401A.
Better assemble a 2nd , or a 3rd LTZ1000 reference, to get a really good voltage baseline.
 
My whole story is on the cited LTZ1000 thread, you may better look there.

Causes of these dips might be from switch mode PSUs, either in LED lighting, (noisy) PC PSUs, cellular phones, WLAN, BT, and so on, even from ordinary glitches in your mains supply, from coffee machines, washing, machines, and so on.

I operate all of my 7 LTZ1000 references down in the basement, there is only old school 50Hz incandescent, or fluorescent light, and a lot of concrete with steel armour around.
Anyhow, only additional shielding measures (tuner box instead of aluminium), ferrite rings and of course some blocking capacitors in the right places (Andreas design) mitigate such glitches to zero.

Frank 
 
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Offline TiN

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Re: KX Reference
« Reply #248 on: April 01, 2020, 05:43:50 am »
grizewald
Very nice write-up, thanks for sharing.

As of jumpy reference. It was one particular reference chip that I talked about. (Out of 30+ various LTZ references I've built total). I don't believe that jumps is something related to LTZ1000ACH version specifically. I mostly use ACH because it is easier to deal with and have much more linear and predictable TC, didn't meet other jumper yet.

That jumpy chip came from eBay A9 3458A board, that I originally bought for my second 3458. After desoldering chip from A9 board and putting onto my KX - it was confirmed that chip itself caused jumps. I tried various things to try mitigate the jumps, but to no avail. Obviously after replacing chip no jumps were present in original design.

Perhaps easy test would be to monitor reference for few days using battery power (such as car/motorcycle 12V battery) inside a shielded can. You can use large cooking can with drilled hole for short shielded cable (or two coax cables) to DMM. This would eliminate possible ground loop currents and power supply noise interference.

Another thing to eliminate the DMM , which can have own jumpy LM399 inside. So for that you can connect both references in opposition and monitor difference with 34401A. Then jumps from DMMs ref could cause much less change, when you just measure few millivolts of difference between REF1 and REF2, and you'd be comparing amplified by 100 input vs internal ppm-level jumps of base 10V range.

« Last Edit: April 01, 2020, 05:46:21 am by TiN »
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Offline Dr. Frank

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Re: KX Reference
« Reply #249 on: April 01, 2020, 10:20:45 am »
Just a reminder, that somebody else already has given this hint:
https://www.eevblog.com/forum/metrology/ultra-precision-reference-ltz1000/msg1879310/#msg1879310

Last year, I measured two A version references, for minimizing their T.C.s and I also saw these 0.5ppm shifts.
Maybe I show these measurements elsewhere.
Frank
 

Offline grizewald

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Re: KX Reference
« Reply #250 on: April 01, 2020, 12:48:40 pm »
Thanks for the great advice Dr. Frank and TiN.

I wish I had a basement, but that's just a dream for us apartment dwellers. :)

I would not even dream of powering the references with a switched mode PSU! They are powered from my Thurlby PL320 linear supply:



I think I have a suitable metal tin to create a shielded environment for the reference and I should also be able to fit some LiPo battery packs in there to provide power for it. That will go a long way towards removing RFI influences. I just need to get some more screened PTFE cable as I seem to have run out.

I let the log continue running and got one huge -80ppm jump last night as shown in the plot below:



When that happened, I took my wireless environmental monitor and relocated it to the other side of the room. This forced me to restart my logging script as the subtask which adds the data from the sensor stopped updating when I had to unplug the sensor to move it. It is interesting to see what happened to the 34401A's readings after I restarted the script. If you look at the plot just after the -80ppm spike, there's a change in the logged voltage back to the 0ppm difference level when I restarted the script (which starts with a *RST command).

It looks like there was something causing an offset to the readings which got cleared when I reset the meter. By default, the 34401A should be performing an auto zero on every reading with the settings I am using, so either that's not true (and I will change the script to turn on auto zero explicitly), or there's some other offset source accumulating in the meter which isn't accounted for by the auto zero.

I hope it is caused by auto zero not being on by default. If it's not, and there's some other kind of offset building up over time, it kind of shakes my confidence in the 34401A for long term logging.
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Re: KX Reference
« Reply #251 on: April 02, 2020, 03:51:53 am »
I am about to populate a couple of these boards to add to the fleet. What is the best current thoughts on enclosures? I have a small stash of these metalised ones or should I stick to a full Aluminium one? Also still foam support or make some 3D printed supports around the perimeter of the board?

TIA  :)
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Offline Andreas

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Re: KX Reference
« Reply #252 on: April 02, 2020, 04:31:50 am »
Hello,

I personally prefer massive metal cases: how do you want to connect a "guard" to your metallisation.
Usually a metallisation is at best a electrostatic shield (for DC) or very high frequencies in the 10 GHz range.

A real shield should have a minimum thickness of 0.5 mm.
Of course you are free to put a Teko steel enclosure (tuner box) within the plastic cabinet.

https://www.reichelt.de/index.html?ACTION=446&LA=0&nbc=1&q=teko%20steel

with best regards

Andreas
 
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Offline BU508A

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Re: KX Reference
« Reply #253 on: April 02, 2020, 07:16:41 am »
Hello,

seems this link to Reichelt doesn't produce any results.

This one might work.
Click on the left side for "Steel sheet housing"
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Re: KX Reference
« Reply #254 on: April 02, 2020, 12:52:58 pm »
As Andreas sayd, effective shielding is a must. The Teko's 373.16 are tinned steel, but the binding posts likely to become a little wobbly. So best for me are the Hammond 1590 aluminium alloy or the HM971-ND. Some pictures because of the space requireds.
 

Offline grizewald

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Re: KX Reference
« Reply #255 on: April 04, 2020, 08:02:14 am »
It looks like there was something causing an offset to the readings which got cleared when I reset the meter. By default, the 34401A should be performing an auto zero on every reading with the settings I am using, so either that's not true (and I will change the script to turn on auto zero explicitly), or there's some other offset source accumulating in the meter which isn't accounted for by the auto zero.

I hope it is caused by auto zero not being on by default. If it's not, and there's some other kind of offset building up over time, it kind of shakes my confidence in the 34401A for long term logging.

I'll quote myself just in case anyone else runs into this.

When setting up the 34401A for logging on 10V DC, maximum resolution and NPLC 100, you could be forgiven for thinking that auto zero would be on by default. The 34401A user manual says that auto zero is enabled for CONF and MEAS when NPLC >= 1.



So I used the following commands to configure my meter:

*RST
*CLS
CONF:VOLT:DC 10, MAX
VOLT:DC:NPLC 100
INP:IMP:AUTO ON

The problem is, that contrary to what the manual tells you, auto zero is NOT on by default with these settings! So, if you think what you are measuring seems to be drifting more than expected, add the line below to your list of commands and auto zero will finally be on. (I added it after the last line in the list above.)

ZERO:AUTO ON

You will know it has worked as the time between each reading will be four seconds instead of two.
« Last Edit: April 04, 2020, 08:08:28 am by grizewald »
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