For calibration, read the 1693 instruction, too. The procedure is ah ... very interesting.
If your 1689 still has the calibration only check your calibration resistors with mean value and highest averaging (measure Q in ppm, write down both values) . If you realize one of the calibration resistors in the meter has drifted out of tolerance, only recalibrate this range with the R-Value from the Ohmmeter and the Q-Value from the check measurement. The Q value does not drift significant, as it is based on the construction of the internal reference, the pcb layout and the like.
Do NOT try to calibrate if avoidable. It will not get better and to reach the same level is very hard work.
Calibration:
FIRST: Start with the frequency calibration.
I used the Q factors from a genrad calibration certificate, until i can measure it better (see Q values below).
i just use 4 bare Vishay Precision resistors, there is no need to have exact the manual values, in fact in the 1689 the reference resistors are used in series, so the sum values are better. I just measured them with my best ohmmeter. Therefore the parts tolerance doesn`t matter. But I use the Vishay because of their very low temperature coefficient. Standard resistors with 100 ppm/°C are not my liking there. So cheaper vishays with e.g 0.1% tolerance are fine.
R= 25 Ohm Q = 11 ppm. Y169025R0000T9L is a four wire shunt resistor upto 8W. For the desktop variant i put a piece of paper between the legs, so each of the 4 legs makes only contact to one electrode, so a perfect Kelvin connection. The inner contacs are bend outwards, so they clip the paper with the 2 outer ones (see picture)
R= 400 Ohm Q = 0 ppm Y0007400R000V0L
R= 6K Q = 2 ppm in use: 1k + 5k soldered together, so that i can use all 3 values (if i need a 1k or a 5k) Y14531K00000T9L and Y14535K00000V9L
R= 100k Q = -258 ppm Check this value with your lowest D Foil capacitor, eg. a X2 type, should be arround 100 ppm. D of capacitors is never negative.
Of course make all measurements with correct open short calibration. For checking the open short must be done for each frequency extra. (eg the hp 4274a / 4275a does it for all frequencies at once and no special code, just 2 buttons)
I checked it against a genrad 1404 100 pF vacuum capacitor, which has D < 10 ppm according to the article in genrad experimenter Aug 1963 page 8.
The procedure for it was really annoying, as i use different cable sets and had to make open and zero calibration when changing between the 100k and the 100pF. I was tweeking the Q of the 100k resistor until the D of the capacitor was at 10 ppm.
This is useful to measure low D foil capacitors.
On picture: pins of 6 k resistor in 60° positions: 1k - 5k - 6k, all 3 values are usable
25 Ohm kelvin resistor pins bent to paperclip for kelvin connection in desktop 1689
short consists of a piece of 1,5 mm² wire flatened with a vice with flat surface. This is ok for 4 wire connection.
