Author Topic: Removing tarnish from high voltage high vacuum feedthrough  (Read 827 times)

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Offline ChristofferBTopic starter

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Removing tarnish from high voltage high vacuum feedthrough
« on: March 03, 2021, 08:30:06 pm »
Hi!

I've just received this really nice NOS MDC vacuum feedthrough. It's a hollow 1/4" copper tube insulated through the vacuum flange by about 18mm of ceramic insulator.

I guess its hollow for high powered applications where the electrodes themselves has cooling water running in them. I'm unsure. I'm gonna seal it with a blob of Sn/Ag solder.

Either way, how would one go about removing the copper tarnish? Abrasives are bad, as fine particles are difficult to get rid of.

Maybe dilute hydrochloric acid or 30% acetic acid?

I'm worried about galvanic corrosion, and deterioration of the metal/ceramic seal...

Also, could anyone venture a guess on the max operating voltage?

Thanks in advance!
--Christoffer //IG:Chromatogiraffery
Check out my scientific instruments diy (GC, HPLC, NMR, etc) Channel: https://www.youtube.com/channel/UCZ8l6SdZuRuoSdze1dIpzAQ
 

Offline Tomorokoshi

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Re: Removing tarnish from high voltage high vacuum feedthrough
« Reply #1 on: March 03, 2021, 09:05:53 pm »
That's tricky because of the special conditions. Perhaps one of the Deoxit series:

https://caig.com/
 

Offline ChristofferBTopic starter

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Re: Removing tarnish from high voltage high vacuum feedthrough
« Reply #2 on: March 03, 2021, 09:28:16 pm »
That could be, I will look for an equivalent brand in the EU. Thanks!

Either way I will try not to expose the ceramic. The inside of the tube could be cleaned by just pushing liquid through a hose attached on each end, and the outside ends with a rag.

--Christoffer //IG:Chromatogiraffery
Check out my scientific instruments diy (GC, HPLC, NMR, etc) Channel: https://www.youtube.com/channel/UCZ8l6SdZuRuoSdze1dIpzAQ
 

Offline vindoline

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Re: Removing tarnish from high voltage high vacuum feedthrough
« Reply #3 on: March 04, 2021, 12:11:09 am »
Chris, it's not clear to me why you want to clean the copper. However, since you're a chemist, you can brush on a solution of sodium chloride and citric acid. That will strip the oxide off the copper.   I don’t imagine it will effect the copper/ceramic junction.
 


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