I know a little about the cooler refill process that I learnt whilst considering a DIY version for my coolers.
1. The process requires UHP Helium, nothing of lesser purity is acceptable.
2. A dryer may be required for the UHP Helium but I am uncertain whether this is essential if quality UHP Helium is sourced.
3. Suitable Helium rated Helium cylinder regulator, gas gauges and hoses are required.
4. A special cryo-cooler fill port adapter is needed to access the sealing screw whilst the port is under pressure. more on that later.
5. A suitable Indium seal is needed to replace the original fitted in the cryo-cooler fill port.
The fill port adapter…..
The fill port on the cryo-cooler is a threaded hole at the bottom of which is a sealing surface against which the sealing screw compresses the Indium seal. The fill port May, or may not have a cover screw inserted to keep dirt out of the port. The cover screw and sealing screw are removed to access the fill port and the indium seal is extracted. At this point all Helium will obviously be vented to atmosphere. The Helium is replaced with whatever gas surrounds the cooler, most likely atmosphere in DIY applications. The atmospheric cases are considered a pollutant and should be purged as part of the refill process. No further disassembly of the cryocooler is required if a Helium refill is all that is to be done. If any other flanges are opened for inspection purposes, the seals must be renewed when reassembled. A full service is normally carried out in clean room conditions to limit the cryo-coolers exposure to contamination. The glass dewar containing the sensor array is under vacuum but these rarely leak and come up to atmosphere. Vacuum Dewar seal leaks are rare compared to those that have to deal with the Houdini of gases that is Helium.
To fill the cryo cooler with gas the adapter that mates with the coolers fill port must accomplish the following….
1. A Helium gas tight seal to the outer face of the cryo cooler port
2. A suitably sealed integrated tool for the insertion of the threaded sealing plug (the new Indium seals may be positioned in the fill port prior to attaching the fill port adapter)
3. A means to vent Helium gas as part of the cryo-cooler casing gas purge process and also used to flush out atmosphere from the Helium filling hoses and gauges.
4. A safety device to prevent overpressure events in the cooler. This is a safety device to safely release pressure if too great a pressure is applied to the fill system. The UHP cylinder will have a gas regulator and gauges but stuff can go wrong quickly at these pressures and safety is important.
The process to fill the cryo-cooler with UHP Helium varies with who you talk to. Some say that the Cryo-Cooler needs to be attached to a vacuum pump and all atmosphere removed with the vacuum pumping action before the Helium gas is injected into the coolers casing. Others use a Helium purge approach but this does require the deliberate loss of UHP helium through “venting” as part of the purge process. The “vac’ing dow” approach is common in HVAC but gas purging is equally common amongst those working in labs. The process of purging will be detailed here.
1.The first step in filling a Cryo Cooler is the removal of all pollutant gases from the refill gas lines, gauges and, of course the coolers casing. The fill lines may be flushed with the UHP Helium to push atmosphere out of them. The coolers casing is more complex…. It is filled with Helium and then the Helium permitted to leak out whilst more UHP helium is being pushed in to prevent atmosphere re-entering the casing. It’s sounds pretty crude to me and it uses a lot of UHP Helium in the fill-vent-fill-vent process. More research is needed on the exact purge process to achieve the enquired expulsion of atmosphere from the cooler casing. Personally I think the vacuum pump method more professional if the cooler seals are designed to cope with vacuum as well as pressure, which I believe they are. The vacuum process literally sucks the atmosphere and pollutant gases out of the coolers casing and components within. There is the risk of pollutants coming back from the vacuum pump so I believe a special pump is needed, but I know nothing more on that topic.
2. Once the coolers casing has been purged of atmosphere it is “just” a case of injecting the UHP Helium at the correct pressure for the particular Cryo-Cooler. IIRC the common fill pressure is around 200psi. I have previously been told that 200psi is not a very high pressure but having seen the results of a 115psi air compressor reservoir tank explosion in safety lectures I have the utmost respect for any gas at this pressure and all that is exposed to it’s forces. The Cryo cooler casing is a very small volume so not a lot of UHP Helium gas is needed. Far more gas is used in the fill hose and casing purge stages than in the final fill.
3. The integrated seal screw tool is used to seal the cryo-cooler once the correct UHP Helium fill pressure has been achieved. The Indium seal is squashed between the seal screw and the fill port seal surface. These must both be carefully cleaned before the fill process begins to avoid microscopic gas leaks past the Indium seal. Helium gas is called the “Houdini of gases” for good reason. It’s molecule size is so small that it can even escape through some metals if a special sealing coating is not used to prevent such. Soft Indium seals are essential as other seals would present little resistance to Heliums efforts to get past them. It is an amazing gas for Cryo-cooling due to its low freezing point and cooler efficiency improvement, but it is also a PITA due to its small molecule size.
4. A dust cover is normally inserted into the cooler fill port to prevent dirt ingress. This often take the form of a large nylon bolt that is screwed into the port. This is not a secondary gas seal as some might think. If it was missing from the cooler at the start of the process, it is of no great concern in terms of gas leakage but the fill port threads should be carefully cleaned and flushed with IPA prior to removing the sealing screw so as to avoid any solid contaminants entering the coolers casing under the pressure of the new Helium gas fill. It is a very good idea to clean the fill port threads before refilling the cooler anyway.
Testing of the refilled cooler is just a case of listening to the cooling cycle and timing how long it takes to drop into the “maintain” mode. Monitoring of sensor temperature is also possible with some cameras. The cameras manufacturers usually state the nominal time for cooling down to operating temperature but ambient temperature has a small effect on this. A cool down time of 5 minutes is not unreasonable for a freshly filled Cryo-cooler but some take longer (up to 10 minutes) It is important to listen to the cryo-cooler as it operates as its sound can provide a further indication of mechanical health. I love linear type coolers as they are quieter than rotary type coolers so sound more “refined”
They also tend to have a longer mechanical life expectancy due to their lower stresses on the internal components. Linear coolers tend to “buzz” with little to no “rattle” in my experience. Rotary coolers are noisy blighters ! There is a lot going on in a rotary cooler in terns of mechanical movement and changes in forces on bearing surfaces. They have a distinctive raucous rattle that is loud at start and moderates once the cooler reaches operating temperature and the motor RPM reduces. A rotary coolers noise signature is very distinctive and I can listen to one operating and normally tell when it sounds “off”. When they start to get more noisy than normal and/or take too long to reach operating temperature, it is time for a service. Long cooling down times can be due to loss of Helium gas fill pressure but an increase in noise can mean a cooler is approaching the end of its mechanical components life and new components will be required during a service. Inspection of a cryo cooler is not something I am qualified to carry out but I suspect it involves careful inspection of the moving parts and sliding surfaces for evidence of wear and damage. Motor and crank bearings are obvious candidates for replacement during a service but the compressor piston seals and the regenerator may also require replacement due to wear. If the special gas tight coating of the cylinder walls has been damaged, the coolers casing would require specialist refurbishment.
Well I think that is enough for now
Fraser