It's been a week now since my first post.
It took me some time to digest it all. especially the LM399-10V-standard thread.
It's become abundantly clear that when you go over 3 digits or so of precision / accuracy / repeatability / etc, then all sorts of small details become important.
My main goal is not to build a perfect voltage standard, but to design and build some measurement equipment for a low budget, but still very usable and affordable. Similar to the Scullcom series, which I quite like.
I think I first start with some simple power supplies. Maybe just a symmetrical power supply from 2x 18650 with built in protection circuits. Then expand with some ADS1118 ADC on a uC for logging data for a few days. For example, build two uC's with PWM based Reference voltage generators, set them to the same voltage output, and then log drift between them. I also still have to do linearity, noise and drift characterization of the HX711 I've got lying around.
I do have the reference manual with full schematic of an old Kelvin-Varley Fluke reference thingie with oil baths, but I do not have a full schematic of any of the more modern PWM based equipment. some block schematics, those do not have enough details for filtering and such. Can't find a (free) schematic of the Valhalla 2701C. Adret 103 was mostly French (Yuck) only block schematic and no full schematic.
The EDN article for zero-offset active lowpass filtering is also interesting, but putting 200k in series is not good for wanting to measure 5+ digits accurate DC. At the moment I'm leaning much more towards a passive (dampened) LC filter approach. Low DC resistance, High dampening for higher frequencies, and maybe add a double pi for sucking out the PWM base frequency. Passive filter is relatively easy to design, because I do not need a sharp corner frequency nor a very linear response just below the corner. I just want high suppression for frequencies of two orders of magnitude above DC
There is lots of room for experimentation. I've got an old Rigol DS1052E but such scopes (and scopes in general) lack accuracy. The old trick for using an audio card for measuring audio-frequency stuff may still be the best option for a low-budget approach.
I also value the remarks of the 74HCT versus analog switches and the DC reference loading. AD411 are above my budget for a thing like this though. but the remark is important enough to also build some 4053 based variant, put some of the switches parallel and compare differences in DC, charge injection, leakage, asymmetric switching and other things that can introduce non-lineairity. One of the experiments is probably to build both 74HCT and 4053 variants, and compare linearity.
I've thought about pulse density modulation.
It's probably not a good idea for this. DC voltage can be extracted sufficiently with a better passive filter (8 stage LC?) while more flanks introduce more non-linearity.
Static 5V voltage standard IC's are another issue. These things become expensive quickly when you want more stability. My goal would be to have around 10ppm resolution / accuracy and drift per year for an EUR10 total BOM cost (exclusive power supply, PCB), and preferably also with readily available (no vintage) parts.