Thinnest doesn't tell us much. Materials will play into it. Even knowing that, it still offers nothing. You need to measure the torque then provide that detail.
If you like to guess, by all means, fingers work fine. You mentioned early on you have one of the books I read. Have you taken the time to read it? It's a pretty good introduction into how to use a VNA, and is filled with tips. Sadly, I have not found a way to absorb the materials outside of taking the time to read them.
The coax of course is MUCH longer than the connectors. So now the upper frequency has less of an effect on the impedance and we should get the same values if there were no other variables. The fact yours changed so much tells me there are other errors with your setup.
Over-tightening can damage connectors, under-tightening can only mess up measurements.
I found the time of 30 minutes that I let the liteVNA warm up to be too short. The S11 noise floor of my device seems to transition into a steady state between 60 and 90 minutes.
While checking that, I noticed something strange. The S11 trace on the display of the liteVNA and in the Solver64 software did not match when using the exact same sweep parameters. What I mean by that are not some small noise differences, but qualitative shape differences of the curves and an approximately 10dB lower noise floor on the liteVNA display.
I redid the calibration many times to rule out calibration issues to cause this difference, but re-calibrating had no visible effect on this. For cross checking, I downloaded the VNA View Qt software and found that the display there matched the one on the device. So I could simply switch the software while leaving everything else untouched to compare the VNA View and Solver64 software output. The differences were still there, and then they somehow mostly disappeared for the newer calibrations and I could not find the reason for this.

Another thing, I noticed while using the up to 9 GHz range, proposed by joeqsmith, was that the noise floor went up significantly above 6.3 GHz, which is of course to be expected on this device. However, when checking the validity of the different calibrations, I found the ones going up to 9 GHz to be affected by a lot of noise, when viewing the short, open and load conditions in the Smith chart. With the calibrations up to 6.3 GHz these result in a small dot at the expected positions for short, open and load. With the ones up to 9 GHz the result is more like an angry ball of wool. This can be reliably reproduced by re-calibrating and just changing the upper sweep bound between 6.3 GHz an 9 GHz.

It's a wise idea to label the kit with a notice about being drawn and quartered if one rotates the standards while tightening them.
I tend to move things around when using the equipment. This means the cables can end up with a rotation force. If the connectors are not tight and the cable rotates, the two center pins can have rotation. For the cheap cables and connectors, maybe you don't care too much. Maybe if you start using precision parts, you care a little more. I posted some photos from another website showing some high grade HP connectors that were damaged this way. My advice is form good habits.
I have not used QT and don't run the LiteVNA stand alone. That said, it's just some basic math and I would not expect there to be much difference if at all. Of course, this assumes that in all three cases, the errors due to the three calibrations are ZERO. My guess is it is a user problem in not knowing all the fine details, some of which is documented in that large software thread. I'll take a stab at it and say you have not changed Solver64's IFBW to match the LiteVNA's default. I mentioned this in that thread as well as a few videos why I use the wider bandwidth and sacrifice noise for speed. Then there is the isolation.
I've been told I have math errors before. The last time was when using it with waveguides. Again, it is certainly possible there are problems with it. Actually, I know there are as some features I started to work on never panned out. But that basic software is almost two decades old and is used on a regular basis. I've also frequently compared the results with a completely different VNA, cables, standards, software. Even in this thread. What you are describing would be a major problem.
If you do feel there is a problem, you will need to provide enough details for me to reproduce it.
I think, on the cheap liteVNA calibration kit, the most critical factor why not to rotate the pin during insertion would be gold coating abrasion.
I did not intend to imply that there was something wrong in Solver64. I just had the impression that the signals were processed in another way before being displayed. This turned out to be true: I did not set the right IFBW values to get comparable results. Regarding repeatability, I think I am on a good way to finally gain some trust in my measurements.
I remember another user who had a similar problem:
https://www.eevblog.com/forum/rf-microwave/nanovna-custom-software/msg4067353/#msg4067353
Yes, that was the problem, Sweep must be turned on before you start the calibration.
It wasn't in the manual (at least not the parts that I read) and it is the opposite of what the Saver app requires, Saver even gives a warning that the Cal cannot start until you disable the continuous sweep.
I think that makes sense since the Cal procedure wants to take control of a few single sweeps, but obviously you can write code however you want, works just fine when you know how to set it up.
I could get a SMA-M to BNC-F pigtail for putting it between the liteVNA and the test cable.
Calibrating that out would require me to build a BNC-M calibration kit, although I already found an article proving that BNC connectors make poor calibrations standards, it may perhaps be sufficient for my application.
=IF(ISNUMBER(VALUE(RIGHT(A2)));A2;LEFT(A2;LEN(A2)-1)*10^(IFERROR(FIND(RIGHT(A2);"kMGTP")*3;IFERROR(FIND(RIGHT(A2);"munp")*-3;0))))
I have two BNC 50 ohm terminators. All of the ones I have inspected use an axial part. Shown after SOLT, then attaching SMA / BNC adapter and BNC loads. Similar results to what you measured with your setup.
I imagine that the cables mating connector on the test equipment is also custom made to get the return loss they were looking for. I assume also that you have no plans to swap it for a standard BNC or different type all together. I wonder if mixing the parts will cause other issues.
I would have thought in Germany you would have access to all basic components like cable and connectors.
For the TDR/TDT, I attempt to follow HP.
https://www.testunlimited.com/pdf/an/5989-5723en.pdf
Solver 64 uses the same coefficients HP uses. My attempts to make a T-check have not worked out. You don't want a T with an added stub and connector. I think I have documented some of that in the NanoVNA custom software thread.
The main graph does allow you to disable the vertical autoscale. I normally just set the sweep range for what I need. So, locking out the horizontal manual scale was intentional but it could certainly be changed.
Nonetheless I have captured an image of what I mean:
Attached was taken from the paper I previously suggested.
Attached was taken from the paper I previously suggested.Yes, your picture shows exactly what I mean: there, the peaks of the pulse response are exactly at the horizontal positions where the slope of the step function is maximal/minimal. In the screenshot that I took, this does not seem to be the case.
There are many different ways of measuring the impedance of cable, but if I had to choose a methodology that's a good compromise between accuracy, simplicity, and cost, I would use a VNA and the methodology I describe in this video:
Attempt to use this technique with the Pasternak RG58C/U cable. This cable is 3' or 0.9144 meters long. Using their 75/length in meters for fstop, call it 75MHz. They talk about start not critical. 100kHz or lower? I set it to 300k in case I decided to try and replicate with my Agilent (limited to 300k). We are down into the muck, so set the IFBW to 1.3kHz. I had to enable the magnification for the Smith chart so we could see something. Then had to add two more gain ranges.
Again, using low grade standards and ideal model. Yellow showing the load, red is cable + load. I am not sure why they care about the stop frequency rather than maybe just wanting the first cross over? Maybe more data points? If we use the second cross over of 50.5, sqrt (50.5 * 50) - 50.25. The first cross over is at 50.1 giving us 50.05.
Guessing better standards and VNA would help but I think we are just asking too much from the low cost setup.
Having read through the thread again in detail, it looks like joeqsmith and pdenisowski tried to measure a ~50 ohm cable with a 50 ohm load at the far end.
This is not wise, as you will just end up exploring the uncertainties of the test setup if the test load is very similar to the Zo of the cable. It looks like they both used short cables so the first alarm bell should have rung when the crossover point was not at the quarter-wave frequency of the coax cable. They both measured at frequencies that were way too low. 1.7MHz and 8MHz? This is obviously not the quarter-wave frequency of the test cable unless they actually used a really long run of cable?
You are meant to use a test resistance that is some way away from the Zo of the cable. If this means trying several resistances until you find a suitable resistance then so be it.
Maybe read up on a bit of theory about how transmission lines can act as impedance transformers and focus on the special case of the quarter-wave transformer.
For a 50 ohm cable, try using something like a 25R test load at the far end. You can also use something like 100R and just look for the first crossing point on the smith chart.
Normally, if someone wanted to match R1 to R2 they would use a quarter-wave transmission line that had a Zo of sqrt(R1*R2) ohms. However, the idea behind the Zo test method is to just exploit the equation to give Zo because you can define R2 as your test load and then use the VNA to measure R1 at the first crossing of the real axis of the smith chart.
A typical RG58 cable or RG223 cable that is about 3ft long should be a quarter-wave long at about 55MHz. This is roughly where the first crossing should take place for the special Tektronix cable.
Note that the Zo will change with frequency, and if you are trying to measure it to nerdy levels of accuracy, then the Zo will be different at (say) 1MHz, 10MHz, 50MHz and 250MHz. The Zo for a typical 5mm diameter coax cable might be about 52 ohms at 1MHz and the Zo might be closer to 50 ohms up at 250MHz for example.
Note also that the quarter-wave method will have a slight error because of the finite loss in the cable. You can minimise this to some degree by using a test resistance closer to 50 ohms. If you use 39 ohms as the test resistor, then I think the Zo result will be more accurate. However, if you use a test load that is too close to 50 ohms, then you will end up exploring the uncertainty of the whole test setup and you will get flawed results.