Having calibrated the DMM with the LTZ inside in all DCV ranges, I cooled it down from 23°C to 15.8°C.
The reading was -1.9ppm low, which gives an overall TC, w/o ACAL, of about +0.3pp/K.
At cold using ACAL, the reading was +3.7ppm, so I estimate the TC of the resistor network to +0.7ppm/K, and of the LTZ circuit to +0.5ppm/K, if a perfect ACAL compensation is assumed.
At normal r.t., I made many ACALs, one after the other, the readings in all DCV ranges then were always within +/- 1ppm to nominal again, no sign of getting that mysterious offset phenomenon.
If you look at all the stability graphs over several hours, you will always see a -1.. -2ppm decrease of reading in the first 8h, or so.
I first assigned that to a warm -up effect, but that's obviously a drift right after each ACAL, instead.
This behavior was not observed when the instrument was new, and I don't understand why this is happening.
As ACV, ACI and most DCI ranges were off by 2% even after DCV calibration, I re -assembled the LM399, put the box over it, and made another DCV calibration.
Again, many ACALs always brought the DMM back to nominal within 1ppm, w/o any shift.
I cooled it down to 8.1°C, reading w/o ACAL was -14.5ppm, which gives a total of +1ppm/°C.
ACAL brought the reading to - 6ppm of nominal.
That gives an estimate for the resistor network of +0.6ppm/K, and -0.4ppm/K for the LM399.
I made another 12h stability run. Noise was evidently less than the unprotected LM399, about 650nVrms, but it showed some popcorn noise, therefore having about 1.5 times the noise of the LTZ reference.
Therefore the fan, which is blowing to the outside, creates some noise on both references due to air draught, confirming TiNs hint about the blocked fan.
I will later measure the LTZs T.C. directly and if its calculated T.C. is confirmed, I will probably trim it to zero, assemble it into the 34465A and have it completely calibrated.
Myself I'm missing several stimuli, or a 5720A / 5725A to do that on my own.
Frank